Preparation of Highly Dispersed Antimony-doped Tin Oxide Nano-powder via Ion-exchange Hydrolysis of SnCl_4 and SbCl_3 and Azeotropic Drying

YANG Fen; ZHANG Xue-jun; TIAN Fang; WU Xu; GAN Fu-xing

首页> 外文期刊>Chinese journal of aeronautics >Preparation of Highly Dispersed Antimony-doped Tin Oxide Nano-powder via Ion-exchange Hydrolysis of SnCl_4 and SbCl_3 and Azeotropic Drying

【24h】

Preparation of Highly Dispersed Antimony-doped Tin Oxide Nano-powder via Ion-exchange Hydrolysis of SnCl_4 and SbCl_3 and Azeotropic Drying

机译：SnCl_4和SbCl_3的离子交换水解及共沸干燥制备高分散锑掺杂氧化锡纳米粉

获取原文

获取原文并翻译 | 示例

掌桥外文数据库（机构版） >>

开具论文收录证明 >>

文献代查 >>

页面导航

摘要
著录项
相似文献
相关主题

摘要

Antimony-doped tin hydroxide colloid precipitates have been synthesized by hydrolysis of SnCl_4 and SbCl_3 using: (1) an ion-exchange hydrolysis to remove chlorine ions, and (2) isoamyl acetate as an azeotropic solvent to obviate water. The obtained dried powder is of high dispersivity without any need for further grinding. The size and dispersivity of the final particles are investigated with the aid of TG-DTA, BET, XRD and TEM. After having calcined, the antimony-doped tin oxide nanopowder possesses a tetragonal rutile structure with high dispersivity, uniform particles and low hard agglomeration.

机译：锑掺杂的氢氧化锡胶体沉淀物是通过以下方法水解SnCl_4和SbCl_3合成的：（1）进行离子交换水解以去除氯离子，以及（2）乙酸异戊酯作为共沸溶剂以消除水。所获得的干燥粉末具有高分散性，而无需进一步研磨。借助TG-DTA，BET，XRD和TEM研究了最终颗粒的尺寸和分散性。掺锑氧化锡纳米粉经煅烧后，具有四方金红石结构，分散性高，颗粒均匀，硬团聚度低。

著录项

来源
《Chinese journal of aeronautics》 |2007年第2期|p.181-186|共6页
作者
YANG Fen; ZHANG Xue-jun; TIAN Fang; WU Xu; GAN Fu-xing;
展开▼
作者单位

Department of Environmental Engineering, School of Resource & Environmental Science, Wuhan University, Wuhan 430079, China;

展开▼
收录信息
原文格式 PDF
正文语种 eng
中图分类航空;
关键词
antimony-doped tin oxide; ion-exchange; iso-amyl acetate; dispersivity;

机译：锑掺杂二氧化锡离子交换乙酸异戊酯分散性;

相似文献

外文文献
中文文献
专利

1. Preparation of Highly Dispersed Antimony-doped Tin Oxide Nano-powder via Ion-exchange Hydrolysis of SnCl4 and SbCl3 and Azeotropic Drying [J] . YANG Fen, ZHANG Xue-jun, TIAN Fang, 中国航空学报（英文版） . 2007,第002期

机译：SnCl4和SbCl3的离子交换水解及共沸干燥制备高分散锑掺杂氧化锡纳米粉
2. Preparation of Highly Dispersed Antimony-doped Tin Oxide Nano-powder via Ion-exchange Hydrolysis of SnCl4 and SbCl3 and Azeotropic Drying [J] . YANG, Fen, ZHANG, 中国航空学报：英文版 . 2007,第002期

机译：SnCl4和SbCl3的离子交换水解及共沸干燥制备高分散锑掺杂氧化锡纳米粉
3. Preparation of highly dispersed antimony-doped tin oxide nanopowders by azeotropic drying with isoamyl acetate [J] . YANG Fen, ZHANG Xue-jun, WU Xu, Transactions of Nonferrous Metals Society of China . 2007,第3期

机译：乙酸异戊酯共沸干燥制备高分散锑掺杂氧化锡纳米粉体
4. Highly Conducting Nanosized Monodispersed Antimony-Doped Tin Oxide Particles Synthesized via Nonaqueous Sol-Gel Method [C] . Vesna Mueller, Jiri Rathousky, Matthias Rasp, NSTI-Nanotech 2010;NSTI nanotechnology conference and expo;Bio Nanotech 2010;NSTI bio nano conference and expo;Microtech 2010;Microtechnology conference and expo;WCM 2010;Workshop on compact modeling;NSTI nanotech ventures;TechConnect summit;Clean technology . 2010

机译：通过非水溶胶-凝胶法合成的高导电纳米级单分散掺杂锑的氧化锡颗粒
5. Preparation of Highly Dispersed Conductive Metals for Electronic Applications: Silver and Copper [D] . LaPlante, Sylas C. 2012

机译：电子应用中高度分散的导电金属的制备：银和铜
6. Preparation of Highly Dispersed Reduced Graphene Oxide Modified with Carboxymethyl Chitosan for Highly Sensitive Detection of Trace Cu(II) in Water [O] . Sheng Chen, Rui Ding, Xiuling Ma, 2010

机译：羧甲基壳聚糖修饰的高分散性还原氧化石墨烯的制备用于高灵敏度检测水中的痕量铜
7. Preparation of Highly Dispersed Antimony-doped Tin Oxide Nano-powder via Ion-exchange Hydrolysis of SnCl4 and SbCl3 and Azeotropic Drying [O] . YANG Fen, ZHANG Xue-jun, TIAN Fang, 2007

机译：SnCl4和SbCl3的离子交换水解及共沸干燥制备高分散锑掺杂氧化锡纳米粉
8. Drying of Ion-Exchange Resins for Resin-Based Preparation of Nuclear Reactor Fuels [R] . Drago, J. P., Haas, P. A., Million, D. L. 1976

机译：离子交换树脂的干燥用于树脂基核反应堆燃料的制备

Preparation of Highly Dispersed Antimony-doped Tin Oxide Nano-powder via Ion-exchange Hydrolysis of SnCl_4 and SbCl_3 and Azeotropic Drying

摘要

著录项

相似文献

相关主题

期刊订阅