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Preparation and Characterization of NovelFe2O3-Flaky Coated Carbon Fiber by Electrospinning and Hydrothermal Methods

机译:电纺丝-水热法制备新型Fe2O3-鳞片状碳纤维及其表征

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A novel hierarchical nanostructure ofFe2O3-flaky coated carbon fibers was produced by the electrospinning process followed by a hydrothermal technique. First, electrospinning of a colloidal solution that consisted of ferric nitrate and polyacrylonitrile (PAN) was performed to produce PAN nanofibers. Then electrospun nanofiber was stabilized and calcinated in nitrogen at 800°C for 2 h to produce carbon nanofibers (CNFs) which were exploited to produceFe2O3-flaky structure using hydrothermal technique. The as-obtained products were characterized by scanning electron microscopy (SEM) and X-ray diffraction (XRD). The results revealed thatFe2O3flakes were successfully grown on the CNFs substrates, and the coverage ofFe2O3flakes could be controlled by simply adjusting the hydrothermal pH value and time.Fe2O3-flaky coated carbon fibers displayed high photocatalytic activity toward degradation of methyl orange (MO) under visible light irradiation.
机译:通过电纺丝工艺和水热技术制备了Fe2O3薄片状碳纤维的新型分层纳米结构。首先,电纺丝由硝酸铁和聚丙烯腈(PAN)组成的胶体溶液,以生产PAN纳米纤维。然后将电纺纳米纤维稳定化,并在氮气中于800°C下煅烧2 h,以生产碳纳米纤维(CNF),并利用水热技术将其用于生产Fe2O3薄片状结构。所获得的产物通过扫描电子显微镜(SEM)和X射线衍射(XRD)表征。结果表明,Fe2O3薄片在CNFs衬底上成功生长,只需调节水热pH值和时间即可控制Fe2O3薄片的覆盖率。辐射。

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