Synthesis and Application of Poly Ionic Liquid-Based on 2-Acrylamido-2-methyl Propane Sulfonic Acid as Corrosion Protective Film of Steel

Ayman M. Atta; Gamal A. El-Mahdy; Hamad A. Allohedan; Mahmood M. S. Abdullah

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Synthesis and Application of Poly Ionic Liquid-Based on 2-Acrylamido-2-methyl Propane Sulfonic Acid as Corrosion Protective Film of Steel

机译：以2-丙烯酰胺基-2-甲基丙烷磺酸为钢的防腐蚀膜的聚离子液体的合成及应用

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The present work aims to prepare new ionic liquid polymers based on protonation of diethylethanolamine (DEEA) with polymerizable monomers such as 2-acrylamido-2-methyl propane sulfonic acid(AMPS) and acrylic acid (AA). The polymerizable monomer was polymerized without solvent toprepare viscous poly ionic liquid as AMPS/AA-QA. The chemical structure and thermal characteristicsof AMPS/AA-QA were investigated by NMR, DSC and TGA. The wetting characteristics ofAMPS/AA-QA were measured at the steel surface by measuring the contact angles. This workdescribes the successful performance of AMPS/AA-QA as eco-friendly corrosion inhibitors for steel inacidic chloride solution. Corrosion inhibition of steel was carried out by electrochemical techniques.The experimental results reveal that AMPS/AA-QA is efficient mixed type corrosion inhibitors.Inhibition efficiency of 93.7% is reached with 25ppm of AMPS/AA-QA. The Nyquist plots composedof one capacitive loop and its diameter increases with increasing AMPS/AA-QA concentrations. Theadsorption of AMPS/AA-QA on steel surface obeys Langmuir isotherm.

机译：本工作旨在基于二乙基乙醇胺（DEEA）与可聚合单体（例如2-丙烯酸酰胺基-2-甲基丙烷磺酸（AMPS）和丙烯酸（AA））的质子化来制备新型离子液体聚合物。可聚合单体在没有溶剂的情况下聚合为AMPS / AA-QA的粘性聚离子液体。通过NMR，DSC和TGA对AMPS / AA-QA的化学结构和热特性进行了研究。通过测量接触角在钢表面测量AMPS / AA-QA的润湿特性。这项工作描述了AMPS / AA-QA作为用于钢的酸性氯化物溶液的环保型缓蚀剂的成功性能。采用电化学技术对钢进行缓蚀，实验结果表明AMPS / AA-QA是一种有效的混合型缓蚀剂，AMPS / AA-QA的含量为25ppm时，缓蚀率达到93.7％。奈奎斯特图由一个电容性回路组成，其直径随AMPS / AA-QA浓度的增加而增加。 AMPS / AA-QA在钢表面的吸附遵循Langmuir等温线。

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《International Journal of Electrochemical Science》 |2015年第8期|共14页
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Ayman M. Atta; Gamal A. El-Mahdy; Hamad A. Allohedan; Mahmood M. S. Abdullah;
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Synthesis and Application of Poly Ionic Liquid-Based on 2-Acrylamido-2-methyl Propane Sulfonic Acid as Corrosion Protective Film of Steel

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