Synthesis and Properties of Alternating Vinylene-Benzothiadiazole-Based Copolymers with Carbazole and Fluorene Derivatives for Photovoltaic Applications

Ali Mohammed Alsalme; Abdulaziz Ali B. Alghamdi; Ammar Abdul Ghani Q. Alhamdani; Ahmed Iraqi

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Synthesis and Properties of Alternating Vinylene-Benzothiadiazole-Based Copolymers with Carbazole and Fluorene Derivatives for Photovoltaic Applications

机译：光伏应用中含咔唑和芴衍生物的交替乙烯-苯并噻二唑基共聚物的合成及性能

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Three vinylene-benzothiadiazole based alternating copolymers with carbazole, 3,6-difluoro carbazoleand fluorene were prepared via Suzuki coupling polymerisation in the presence of catalytic amounts ofpalladium (II) acetate Pd(OAc)2 and tri-ortho-tolylphosphine. P(o-tol)3. The molecular weightsmeasured by gel permeation chromatography and copolymers were characterised by NMR, UV-Visspectroscopy and cyclic voltammetry. The physical properties and their band gaps are discussed inrelation with their donor units (carbazole and fluorene derivatives).

机译：在催化量的乙酸钯（II）Pd（OAc）2和三邻甲苯基膦存在下，通过Suzuki偶联聚合反应制备了三种基于亚乙烯基-苯并噻二唑的咔唑，3,6-二氟咔唑和芴交替共聚物。 P（邻位）3。用NMR，UV-Visspectroscopy和循环伏安法表征通过凝胶渗透色谱法和共聚物测得的分子量。讨论了其物理性质及其带隙与它们的供体单元（咔唑和芴衍生物）的关系。

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《International Journal of Electrochemical Science》 |2014年第4期|共22页
作者
Ali Mohammed Alsalme; Abdulaziz Ali B. Alghamdi; Ammar Abdul Ghani Q. Alhamdani; Ahmed Iraqi;
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1. Synthesis of new alternating conjugated copolymers consisting of tetrazine/carbazole or tetrazine/fluorene derivatives along with thiophene spacers for photovoltaic applications [J] . Myung-Jin Baek, Wooree Jang, Soo-Hyoung Lee Synthetic Metals . 2011,第23a24期

机译：合成由四嗪/咔唑或四嗪/芴衍生物与噻吩间隔基组成的新型交替共轭共聚物，用于光伏应用
2. Synthesis of new alternating conjugated copolymers consisting of tetrazine/carbazole or tetrazine/fluorene derivatives along with thiophene spacers for photovoltaic applications [J] . Myung-Jin Baek, Wooree Jang, Soo-Hyoung Lee Synthetic Metals . 2011,第23a24期

机译：合成由四嗪/咔唑或四嗪/芴衍生物与噻吩间隔基组成的新型交替共轭共聚物，用于光伏应用
3. Triphenylamine-Fluorene Alternating Conjugated Copolymers with Pendant Acceptor Groups: Synthesis, Structure-Property Relationship, and Photovoltaic Application [J] . Zhang ZG, Zhang KL, Liu G, Macromolecules . 2009,第8期

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4. Synthesis and EL Properties of the Copolymers Derived from Fluorene and Thiophene Derivatives [C] . Qiong China-Japan joint symposium on conduction and photoconduction in organic solids and related phenomena;CJOSS-7 . 2001

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5. Ring opening metathesis polymerization of 1-substituted cyclobutene derivatives and its application to antimicrobials: From homopolymers to alternating copolymers [D] . Song, Airong 2010

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6. Advantageous Microwave-Assisted Suzuki Polycondensation for the Synthesis of Aniline-Fluorene Alternate Copolymers as Molecular Model with Solvent Sensing Properties [O] . Rebeca Vázquez-Guilló, Alberto Falco, M. José Martínez-Tomé, 2018

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7. Impact of fluorine substitution upon the photovoltaic properties of benzothiadiazole-fluorene alternate copolymers [O] . Cartwright, L., Iraqi, A., Zhang, Y., 2015

机译：氟取代对苯并噻二唑 - 芴交替共聚物的光伏特性的影响

Synthesis and Properties of Alternating Vinylene-Benzothiadiazole-Based Copolymers with Carbazole and Fluorene Derivatives for Photovoltaic Applications

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