Solvent-free synthesis of novel 2,10-dichoro-12-trichloromethyl-6-substituted xanthato-12H-dibenzo[d,g] [1,3,2] dioxaphosphocin-6-sulfides

M. Veera Narayana Reddy; G. Chandra Sekhar Reddy; Ch. Syama Sundar; K. Suresh Kumar; K. Ananda Kumar; C. Suresh Reddy

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Solvent-free synthesis of novel 2,10-dichoro-12-trichloromethyl-6-substituted xanthato-12H-dibenzo[d,g] [1,3,2] dioxaphosphocin-6-sulfides

机译：新型2,10-二氯十二-三氯甲基-6-取代的xanthato-12H-二苯并[d，g] [1,3,2]二氧杂膦-6-硫化物的无溶剂合成

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2,10-Dichloro-12-trichloromethyl-6-substituted xanthato-12H-dibenzo[d,g] [1,3,2] dioxaphosphocin-6-sulfides (2a–l) with the eight-membered phosphorus and oxygen heterocyclic ring were synthesized by reacting equimolar quantities of alcohols, carbon disulfide, and 2,6,10-trichloromethyl-12H-dibenzo[d,g][1,3,2] dioxaphosphocin-6-sulfide 1 in the presence of dimethylaminopyridine (DMAP). The structures of the products were confirmed by IR, 1H, 13C, 31P-NMR, and mass spectral analyses.

机译：2,10-二氯-12-三氯甲基-6-取代的xanthato-12H-二苯并[d，g] [1,3,2]二氧磷膦-6硫化物（2a–l）具有八元磷和氧杂环在二甲基氨基吡啶（DMAP）存在下，使等摩尔量的醇，二硫化碳和2,6,10-三氯甲基-12H-二苯并[d，g] [1,3,2]二氧磷膦-6-硫化物1反应合成。产物的结构通过IR，1 H，13 C，31 P-NMR和质谱分析确认。

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《Green Chemistry Letters and Reviews》 |2012年第3期|共5页
作者
M. Veera Narayana Reddy; G. Chandra Sekhar Reddy; Ch. Syama Sundar; K. Suresh Kumar; K. Ananda Kumar; C. Suresh Reddy;
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中图分类化学;
关键词
dibenzodioxaphosphocin monochloride4-dimethylaminopyridinedioxaphosphocin-6-sulfidexanthates;

机译：二氯化二苯并二氧杂膦酸4-二甲氨基吡啶二氧杂膦-6-硫代黄原酸酯;

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1. Solvent-free synthesis of novel 2,10-dichoro-12-trichloromethyl-6-substituted xanthato-12H-dibenzo[d,g] [1,3,2] dioxaphosphocin-6-sulfides [J] . M. Veera Narayana Reddy G. Chandra Sekhar Reddy Ch. Syama Sundar K. Suresh Kumar K. Ananda Kumar, C. Suresh Reddy Green Chemistry Letters and Reviews . 2012,第3期

机译：新型2,10-二氯十二-三氯甲基-6-取代的黄原-12H-二苯并[d，g] [1,3,2]二氧膦-6硫化物的无溶剂合成
2. Electron impact mass spectra of 6-substituted 12H-tetrachlorodibenzo[d,g][1,3,2] dioxaphosphocin-6-sulfides and oxides [J] . Li CJ., Fei J., Chen WY., Rapid Communications in Mass Spectrometry: RCM . 2000,第14期

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4. Synthesis of 2-Ethoxy-5,5-Dimethyl-1,3,2-Dioxaphosphinane 2-Oxide [C] . Xinye Zhao, Huizhen Zhi, Jinfei Yang International symposium on flame-retardant materials technologies . 2018

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Solvent-free synthesis of novel 2,10-dichoro-12-trichloromethyl-6-substituted xanthato-12H-dibenzo[d,g] [1,3,2] dioxaphosphocin-6-sulfides

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