Synthesis and structural studies of Glucosylimino-1,2,4,5-Tetrazine

B. N. Berad; S. M.Bhiwagade; A. G. Ulhe

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Synthesis and structural studies of Glucosylimino-1,2,4,5-Tetrazine

机译：1,2,4,5-四氢葡萄糖苷的合成与结构研究

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Series of 3-tetra-O-acetyl–β-D-glucopyranosylimino, 6 substituted -1,2,4,5-tetrazine (IV) have been synthesized by the reaction of aryl dihydroformazanes (III) and tetra-O-acetyl-β-D-glucosylimino-isocyanodichloride in refluxing chloroform medium. The aryl dihydroformazans (III) were prepared by the interaction of acid hydrazides (I) and hydrazine hydrate (II) in refluxing ethanol medium in 1:1 proportion. The structures of tetrazines (IV) were confirmed on the basis of elemental analysis and IR, PMR, 13C and mass spectral analysis.

机译：通过芳基二氢甲氮烷（III）与四-O-乙酰基-四氢呋喃的反应合成了一系列3-四-O-乙酰基-β-D-吡喃葡萄糖基嘧啶（6）取代的1,2,4,5-四嗪（IV）。回流氯仿介质中的β-D-葡萄糖基亚氨基-异氰基二氯化物。酰肼（Ⅰ）和水合肼（Ⅱ）在回流的乙醇介质中以1：1的比例反应制得芳基二氢甲酰胺（Ⅲ）。在元素分析，IR，PMR，13C和质谱分析的基础上确认了四嗪（IV）的结构。

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《Der Pharma Chemica: journal for medicinal chemistry, pharmaceutical chemistry and computational chemistry》 |2012年第4期|共5页
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B. N. Berad; S. M.Bhiwagade; A. G. Ulhe;
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Synthesis and structural studies of Glucosylimino-1,2,4,5-Tetrazine

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