Mild and efficient method for oxidation of alcohol to carboxylic acid followed by synthesis of amide analogues of Coreya??s lactone

K. Venkata Rambabu; G. Mahesh Reddy; K. Mukkanti

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Mild and efficient method for oxidation of alcohol to carboxylic acid followed by synthesis of amide analogues of Coreya??s lactone

机译：温和有效的方法，将醇氧化为羧酸，然后合成Coreya的内酯酰胺类似物

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A mild, safe and efficient method for the oxidation of Corey’s lactone to carboxylic acid under modified Anelli’s oxidation condition has been developed. The oxidation reaction proceeded at room temperature under biphasic reaction in DCM/water with high yield. Further, treatment of carboxylic acid with various amines was studied for the first time, resulting in the formation of amides in good to excellent yields.

机译：开发了一种温和，安全，有效的方法，用于在改良的Anelli氧化条件下将Corey的内酯氧化为羧酸。氧化反应在室温下在DCM /水中的双相反应下以高收率进行。此外，首次研究了用各种胺处理羧酸的方法，从而形成了产率高至优异的酰胺。

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《Der Pharma Chemica: journal for medicinal chemistry, pharmaceutical chemistry and computational chemistry》 |2012年第1期|共7页
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K. Venkata Rambabu; G. Mahesh Reddy; K. Mukkanti;
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1. Oxidation of alcohol to carboxylic acid under mild acidic condition and followed by synthesis of ester analogues of Corey's lactone [J] . Venkata Rambabu Kammili, G. Mahesh Reddy, K. Mukkanti Der Pharma Chemica: journal for medicinal chemistry, pharmaceutical chemistry and computational chemistry . 2011,第5期

机译：在弱酸性条件下将醇氧化成羧酸，然后合成科里内酯的酯类似物
2. Inter- and Intramolecular Addition Reactions of Electron-Deficient Alkenes with Alkyl Radicals, Generated by SET-Photochemical Decarboxylation of Carboxylic Acids, Serve as a Mild and Efficient Method for the Preparation of gamma-Amino Acids and Macrocyclic Lactones [J] . Yoshimi Y, Masuda M, Mizunashi T, Organic letters . 2009,第20期

机译：SET-光化学脱羧羧酸产生的电子缺陷型烯烃与烷基自由基的分子间和分子内加成反应，是一种温和高效的制备γ-氨基酸和大环内酯的方法
3. Condensation Between Isocyanates and Carboxylic Acids in teh Presence of 4-Dimethylaminopyridine (DMAP),a Mild and Efficient Synthesis of Amides [J] . Anne C.Schumacher, R.W.Hoffmann Synthesis: International Journal of Methods in Synthetic Organic Chemistry . 2001,第0期

机译：4-二甲基氨基吡啶（DMAP）存在下异氰酸酯与羧酸之间的缩合，酰胺的轻度高效合成
4. Synthesis of Carboxylic Acids Intercalated Mg-Al Layered Double Hydroxides by a Modified Reconstruction Method [C] . Weidong Yang, Sheng Li, Dong Yang Wu, International Symposium on Advanced Synthesis and Processing Technology for Materials . 2009

机译：改性重建方法合成羧酸嵌入式Mg-Al层双氢氧脂
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6. Microwave-Assisted Catalytic Method for a Green Synthesis of Amides Directly from Amines and Carboxylic Acids [O] . Adam P. Zarecki, Jacek L. Kolanowski, Wojciech T. Markiewicz 2020

机译：微波催化直接由胺和羧酸绿色合成酰胺的微波催化方法
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Mild and efficient method for oxidation of alcohol to carboxylic acid followed by synthesis of amide analogues of Coreya??s lactone

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