Synthesis and characterization tris N-2,4-dinitrophenyl N/-3-nitrobenzylidenehydrazine palladium chloride and tris N-2,4- dinitrophenyl N/-3-phenyl alilidine hydrazine

Mohamad Mehdi Akbarzade; Ali Naderi

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Synthesis and characterization tris N-2,4-dinitrophenyl N/-3-nitrobenzylidenehydrazine palladium chloride and tris N-2,4- dinitrophenyl N/-3-phenyl alilidine hydrazine

机译：tris N-2,4-二硝基苯基N / -3-硝基苄叉肼氯化钯和tris N-2,4-二硝基苯基N / -3-苯基丙啶肼的合成和表征

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The reaction between two acetohydrazide ligands that are, N-2,4dinitrophenyl N/-3-nitrobenzylidenehydrazine and Tris N-2,4dinitrophenyl N/-3-phenyl alilidinehydrazine with PdCl2 produced two new ionic palladium complexes. One of them is TNBH which is easily synthesized in a nearly quantitative yield using a direct reaction between PdCl2 and N-2,4dinitrophenyl N/-3-nitrobenzylidenehydrazine. Another is TDPH which has been synthesized by the reaction of Tris N-2,4dinitrophenyl N/-3-phenyl alilidinehydrazine with PdCl2. These compounds are characterized by spectroscopic techniques. The electronic and vibrational spectra of TDPH and TNBH have been measured and studied.

机译：N-2,4-二硝基苯基N / -3-硝基苄基亚甲基肼和Tris N-2,4-二硝基苯基N / -3-苯基丙啶肼的两个乙酰肼配体与PdCl2的反应产生了两个新的离子钯配合物。其中之一是TNBH，使用PdCl2与N-2,4-二硝基苯基N / -3-硝基苄基亚甲基肼之间的直接反应，可以很容易地以接近定量的产率合成。另一个是TDPH，它是通过Tris N-2,4二硝基苯基N / -3-苯基丙啶肼与PdCl2反应合成的。这些化合物通过光谱技术表征。对TDPH和TNBH的电子和振动光谱进行了测量和研究。

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《Der Pharma Chemica: journal for medicinal chemistry, pharmaceutical chemistry and computational chemistry》 |2014年第1期|共5页
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Mohamad Mehdi Akbarzade; Ali Naderi;
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Synthesis and characterization tris N-2,4-dinitrophenyl N/-3-nitrobenzylidenehydrazine palladium chloride and tris N-2,4- dinitrophenyl N/-3-phenyl alilidine hydrazine

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