Efficient Ultrasound synthesis of ?2-diketone and its metal complexes

Anjali S. Rajbhoj; a S Korde; Suresh T. Gaikwad; Seema S. Korde

首页> 外文期刊>Der Pharma Chemica: journal for medicinal chemistry, pharmaceutical chemistry and computational chemistry >Efficient Ultrasound synthesis of ?2-diketone and its metal complexes

【24h】

Efficient Ultrasound synthesis of ?2-diketone and its metal complexes

机译：超声有效合成β2-二酮及其金属配合物

获取原文

掌桥外文数据库（机构版） >>

开具论文收录证明 >>

文献代查 >>

页面导航

摘要
著录项
相似文献
相关主题

摘要

1-(5-chloro,2-hydroxyphenyl)-3-(4-ethoxyphenyl)propane-1,3-dione and its transition metal complexes have been synthesized by ultrasound irradiation method. The diketone is offered by employing Baker-Venkatraman rearrangement on 5-chloro, 2-acetylphenyl,4-ethoxy benzoate. The synthesized compounds were confirmed by the spectroscopic analysis such as IR, 1H-NMR, 13C-NMR ,Mass, Elemental analysis, magnetic susceptibility and evaluated for antimicrobial screening.

机译：通过超声辐照合成了1-（5-氯，2-羟基苯基）-3-（4-乙氧基苯基）丙烷-1,3-二酮及其过渡金属配合物。通过在5-氯，2-乙酰基苯基，4-乙氧基苯甲酸酯上使用贝克-文卡特拉曼重排来提供二酮。合成的化合物通过IR，1 H-NMR，13 C-NMR，质谱，元素分析，磁化率等光谱分析确认，并进行了抗菌筛选。

著录项

来源
《Der Pharma Chemica: journal for medicinal chemistry, pharmaceutical chemistry and computational chemistry》 |2012年第5期|共5页
作者
Anjali S. Rajbhoj; a S Korde; Suresh T. Gaikwad; Seema S. Korde;
展开▼
作者单位

展开▼
收录信息
原文格式 PDF
正文语种
中图分类化学;
关键词

相似文献

外文文献
中文文献
专利

1. Efficient Ultrasound Synthesis, Spectral studies of 1-(2-hydroxyphenyl)-3-(4-nitrophenyl) propane-1, 3-dione with metal complexes as antibacterial and antifungal agents [J] . Dayanand M. Suryawanshi, Vijayanand D. Ingale, Anjali S. Rajbhoj, Research Journal of Chemical Sciences . 2016,第11期

机译：高效超声波合成，1-（2-羟苯基）-3-（4-硝基苯基）丙烷-1,3-二酮与金属配合物作为抗菌和抗真菌剂的光谱研究
2. Ultrasound-assisted synthesis of aromatic 1,2-diketones from oximinoketones under neutral conditions in aqueous media [J] . Mehrabi H. Ultrasonics sonochemistry . 2012,第1期

机译：在水性介质中性条件下由肟基酮超声辅助合成芳香族1,2-二酮
3. Transition-Metal Complexes with Singly Reduced 1,2-Diketone Radical Ligands [J] . Geoffrey H. Spikes, Eckhard Bill, Thomas Weyhermuller Angewandte Chemie . 2008,第16期

机译：1,2-二酮自由基配体的过渡金属配合物
4. Catalytic Addition of Amines to Carbon Monoxide by Rare Earth Metal Complexes : An Efficient Synthesis of N-Substituted Formamides [C] . Toshiaki Suzuki, Zhaomin Hou Symposium on Organometallic Chemistry . 2008

机译：通过稀土金属配合物催化添加胺至一氧化碳：高效合成N-取代的甲酰胺
5. Ethylene-bis(indenyl) catalytic complexes: Efficient synthesis, introduction of the active metal species and immobilization. [D] . Panarello, Anthony P. 2005

机译：乙烯-双（茚基）催化络合物：高效合成，活性金属种类的引入和固定化。
6. Hydroxynaphthoquinone Metal Complexes as Antitumor Agents X: Synthesis Structure Spectroscopy and In Vitro Antitumor Activity of 3-Methyl-Phenylazo Lawsone Derivatives and Their Metal Complexes Against Human Breast Cancer Cell Line MCF-7 [O] . Nikhil Gokhale, Subhash Padhye, Chris Newton, 2000

机译：羟基萘醌金属配合物作为抗肿瘤剂X：3-甲基苯基偶氮唑烷酮及其金属配合物对人乳腺癌细胞MCF-7的合成结构光谱和体外抗肿瘤活性
7. Efficient New Synthetic Route to Bidentate, Monomeric Cyclopentadienyl-Amide Complexes of Group 4 Transition Metals: Synthesis and Characterization of the Zirconium and Hafnium Complexes [{η5 [O] . Hughes, Andrew K., Meetsma, Auke, Teuben, Jan H. 1993

机译：有效的新合成路线，以鉴定第4组过渡金属的单体环戊二烯基-酰胺配合物：锆和Ha配合物的合成和表征[{η5
8. Chemistry of Polynuclear Metal Complexes with Bridging Carbene or Carbyne Ligands. Part 90. (1) Synthesis of the Complexes (W2M2(mu-CO)(mu-CMe)(mu3-CMe)-(Mu-PPh2)2(CO)3(eta-C5H5)2) (M = Rh or Ir) and Related Tetra- and Penta-nuclear Metal Compounds: Interconversion of Ketenyl and Lambda(5) -Phospha-alkyne Ligands Bridging Tungsten-Rhodium Bonds. [R] . Davies, S. J., Stone, F. G. 1989

机译：具有桥接卡宾或卡宾配体的多核金属配合物的化学。部分90.（1）配合物的合成（W2m2（mu-CO）（mu-Cme）（mu3-Cme） - （mu-pph2）2（CO）3（eta-C5H5）2）（m = Rh或Ir）和相关的四核和五核金属化合物：Ketenyl和Lambda（5）-phospha-alkyne配体桥联钨 - 铑键的相互转化。

Efficient Ultrasound synthesis of ?2-diketone and its metal complexes

摘要

著录项

相似文献

相关主题

期刊订阅