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外部拡散法MgB2線材の組織と超伝導特性

机译:外部扩散法MgB2线的结构和超导性能

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MgB_(2) wires have been prepared by diffusion process using pure Mg metal tube. Amorphous B powder mixed with 5 mol% SiC nano-sized powder addition was encased in a Mg tube, and then the tube was inserted into a pure iron tube to form the Fe/Mg/B(powder) composite wires. The composite was drawn into around wires of 1.0 ~ 0.8 mm in diameter without intermediate annealing. The composite wires were heat treated at 630 °C for 5 h in Ar gas atmosphere. Some of the specimens were hot-pressed under 10 MPa during heat treatment. The MgB_(2) core was synthesized through the diffusion reaction between outside Mg metal tube and inside B powder with SiC addition. The MgB_(2) core forms denser structure without voids and cracks in comparison with conventional in-situ PIT processed MgB_(2) wires. The Ic values at 4.2 K for the MgB_(2) wire of 1.0 mm and 0.8 mm in diameter reaches to 134 A and 187 A at 5 T ,which corresponds to the Jc of 2230 A/mm~(2) and 3740 A/mm~(2), respectively. The Ic of the hot-pressed wire is 164 A at 5 T.
机译:MgB_(2)线是通过使用纯Mg金属管的扩散工艺制备的。将混合有5 mol%SiC纳米粉末的非晶B粉末装入Mg管中,然后将其插入纯铁管中以形成Fe / Mg / B(粉末)复合丝。将复合材料拉成直径为1.0〜0.8 mm的金属丝,而无需中间退火。在Ar气氛中将复合线材在630°C热处理5 h。在热处理过程中,一些样品在10 MPa下被热压。 MgB_(2)核是通过在外Mg金属管和内B粉末之间添加SiC进行扩散反应而合成的。与传统的原位PIT处理的MgB_(2)导线相比,MgB_(2)芯形成的致密结构没有空隙和裂纹。直径为1.0 mm和0.8 mm的MgB_(2)线在4.2 K时的Ic值在5 T时分别达到134 A和187 A,相当于Jc为2230 A / mm〜(2)和3740 A /毫米〜(2) 5 T时,热压丝的Ic为164A。

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