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首页> 外文期刊>Digest Journal of Nanomaterials and Biostructures >SYNTHESIS OF HEXADECYLAMINE CAPPED ZnO NANOPARTICLES USINGBIS(2-HYDROXY-1-NAPHTHALDEHYDATO)ZINC(II) AS A SINGLE SOURCEPRECURSOR
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SYNTHESIS OF HEXADECYLAMINE CAPPED ZnO NANOPARTICLES USINGBIS(2-HYDROXY-1-NAPHTHALDEHYDATO)ZINC(II) AS A SINGLE SOURCEPRECURSOR

机译：以双（2-羟基-1-萘代乙二醛）锌（II）为单源合成六环嘧啶包覆的ZnO纳米粒子

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摘要

Salicyladehyde and 2-hydroxy-1-naphthaldehyde were used as ligands to preparebis(salicylidene)zinc(II) and bis(2-hydroxy-1-naphthaldehydato)zinc(II) complexes. Thebis(2-hydroxy-1-naphthaldehydato)zinc(II) complex was used as a precursor to synthesizezinc oxide nanoparticles via thermal decomposition technique at different temperaturesusing hexadecylamine (HDA) as a stabilizing agent. The results show that decompositiontemperature has a huge effect during the formation of the ZnO nanomaterials. The TEMimages of the as synthesized nanoparticles revealed different shapes of the particles as thedecomposition temperature was increased from 145 to 190 °C. The diffraction patterns ofall ZnO nanoparticles synthesized at various temperatures show hexagonal structures withthe lattice parameter of a = b = 3.25 ? and c = 5.20 ?.
机译：以水杨醛和2-羟基-1-萘醛为配体制备双（水杨基）锌（II）和双（2-羟基-1-萘二氢）锌（II）配合物。以十六烷基胺（HDA）为稳定剂，在不同温度下通过热分解技术，以双（2-羟基-1-萘二氢）锌（II）络合物为前驱体合成氧化锌纳米颗粒。结果表明，分解温度对ZnO纳米材料的形成有很大的影响。随着分解温度从145°C升高到190°C，合成的纳米颗粒的TEM图像显示出不同形状的颗粒。在不同温度下合成的所有ZnO纳米粒子的衍射图样均显示出六边形结构，其晶格参数为a = b = 3.25？并且c ＝5.20Ω。

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