Crystal structure of di­chlorido­bis­(4-ethyl­aniline-κN)zinc

Govindaraj J.; Thirumurugan S.; Reddy D.S.; Anbalagan K.; SubbiahPandi A.

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Crystal structure of dichloridobis(4-ethylaniline-κN)zinc

机译：二氯双（4-乙基苯胺-κN）锌的晶体结构

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The title compound, [ZnCl2(C8H11N)2], was synthesized by the reaction of zinc dichloride and 4-ethylaniline. The Zn2+ cation is coordinated by two Cl− anions and the N atoms of two 4-ethylaniline ligands, forming a distorted Zn(N2Cl2) tetrahedron. The dihedral angle between the two benzene rings is 85.3 (2)° The Zn atom lies on a twofold rotation axis. The ethyl substituents are disordered over two sets of sites in a 0.74 (2):0.26 (2) ratio. In the crystal, N—H⋯Cl hydrogen bonds link the molecules into sheets perpendicular to the a axis. C—H⋯Cl interactions also occur.

机译：通过二氯化锌和4-乙基苯胺的反应合成标题化合物[ZnCl2（C8H11N）2]。 Zn2 +阳离子由两个Cl-阴离子和两个4-乙基苯胺配体的N原子配位，形成扭曲的Zn（N2Cl2）四面体。两个苯环之间的二面角为85.3（2）°。Zn原子位于双重旋转轴上。乙基取代基在两组位点上的比率为0.742（2）：0.26（2）。在晶体中，NH 3 Cl氢键将分子连接成垂直于a轴的薄片。 C-HCl相互作用也会发生。

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《Acta Crystallographica Section E: Crystallographic Communications》 |2015年第2期|共页
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Govindaraj J.; Thirumurugan S.; Reddy D.S.; Anbalagan K.; SubbiahPandi A.;
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Crystal structure of di­chlorido­bis­(4-ethyl­aniline-κN)zinc

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Crystal structure of dichloridobis(4-ethylaniline-κN)zinc