Synthesis and characterization of Gd2Zr2O7 defect-fluorite oxide nanoparticles via a homogeneous precipitation-solvothermal method

Zhe Tang; Zhangyi Huang; Jianqi Qi; Xiaofeng Guo; Wei Han; Mao Zhou; Shuting Peng; Tiecheng Lu

首页> 外文期刊>RSC Advances >Synthesis and characterization of Gd₂Zr₂O₇ defect-fluorite oxide nanoparticles via a homogeneous precipitation-solvothermal method

【24h】

Synthesis and characterization of Gd₂Zr₂O₇ defect-fluorite oxide nanoparticles via a homogeneous precipitation-solvothermal method

机译：均相沉淀-溶剂热法合成Gd _{2 Zr _{2 O _{7 缺陷型萤石氧化物纳米粒子及其表征}}}

展开▼

获取原文

免费外文文献都是OA文献，本网站仅为用户提供查询和代理获取服务，本网站没有原文。下单后我们将采用程序或人工为您竭诚获取高质量的原文，但由于OA文献来源多样且变更频繁，仍可能出现获取不到、文献不完整或与标题不符等情况，请知悉并谅解

掌桥外文数据库（机构版） >>

开具论文收录证明 >>

文献代查 >>

免费

页面导航

摘要

著录项

相似文献

相关主题

摘要

Defect-fluorite structured Gd₂Zr₂O₇ nanoparticles were successfully synthesized via a homogeneous precipitation-solvothermal method using urea as a precipitant. The obtained nanoparticles were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), Brunauer–Emmett–Teller (BET) analysis and transmission electron microscopy (TEM). Compared to the traditional solvothermal method, this homogeneous precipitation-solvothermal method has the advantage of producing nanoparticles with small grain sizes, a narrow size-distribution, high surface areas and little agglomeration. Particularly, the mean crystallite size of Gd₂Zr₂O₇ obtained by this method is 20–30 nm, providing a great opportunity of using these nanoparticles as starting nano-sized building blocks for low temperature preparation of homogeneous and dense ceramics. 展开▼

机译：萤石结构的Gd _{2 Zr _{2 O _{7 通过使用尿素作为沉淀剂的均相沉淀-溶剂热法成功地合成了小颗粒。通过X射线衍射（XRD），傅立叶变换红外光谱（FT-IR），扫描电子显微镜（SEM），Brunauer-Emmett-Teller（BET）分析和透射电子显微镜（TEM）对获得的纳米颗粒进行表征。与传统的溶剂热法相比，这种均匀的沉淀-溶剂热法的优势在于可以生产出粒径小，粒度分布窄，表面积大，团聚少的纳米颗粒。特别地，Gd _{2 Zr _{2 O _{7 为20–30 nm，这提供了将这些纳米颗粒用作起始纳米尺寸构建基块用于低温制备均相和致密陶瓷的巨大机会。}}}}}} 展开▼

著录项

来源
《RSC Advances》 |2017年第87期|共6页

作者
Zhe Tang; Zhangyi Huang; Jianqi Qi; Xiaofeng Guo; Wei Han; Mao Zhou; Shuting Peng; Tiecheng Lu;
展开▼

作者单位

展开▼

收录信息

原文格式 PDF

正文语种

中图分类化学;

关键词

相似文献

外文文献

中文文献

专利

1. Synthesis and characterization of Gd2Zr2O7 defect-fluorite oxide nanoparticles via a homogeneous precipitation-solvothermal method [J] . Tang Zhe, Huang Zhangyi, Qi Jianqi, RSC Advances . 2017,第87期

机译：Gd2Zr2O7缺陷 - 氟盐氧化物纳米粒子通过均相沉淀 - 溶剂溶液的合成与表征

2. The Preparation of Nano-oxides of Zinc and Barium of [Ba (o-phen)4] [Zn (EDTA)], [Zn(o-phen)4]2 [ Ba(SCN)6], and Synthesis of ZrO2 Nanoparticles by Chemical Methods [J] . MOHAMMAD HAKIMI, HAMIDEH SARAVANI, ABDOULHAMID ARBABI Oriental Journal of Chemistry: An International Research Journal of Pure & Applied Chemistry . 2018,第3期

机译：锌的纳米氧化物和[BA（O-Phen）4] [Zn（EDTA）]，[Zn（O-Phen）4] 2 [Ba（SCN）6]的制备，以及ZrO2纳米颗粒的合成通过化学方法

3. Room Temperature Synthesis and Characterization of Hybrid Nanoparticles of NiMo over the Surface of Mixed Oxides (Al2O3-TiO2 and Al2O3-ZrO2) Using Ultrasound Radiation [J] . Gholizadeh Elham Morteza, Ghiaci Mehran Catalysis Letters . 2015,第2期

机译：超声辐射在混合氧化物（Al2O3-TiO2和Al2O3-ZrO2）表面上室温合成NiMo杂化纳米颗粒的表征

4. Synthesis and Characterization of La_(0.6)Sr_(0.4)Co_(0.2)Fe_(0.8)O_3 Nanofiber/Ce_(0.9)Gd_(0.1)O_2 Nanoparticle Composite as Cathode Material for Intermediate Temperature Solid Oxide Fuel Cells [C] . C. L. Gao, Y. J. Liu, R. V. Kumar International Symposium on Solid Oxide Fuel Cells . 2013

机译：La_（0.6）Sr_（0.4）Co_（0.2）Fe_（0.8）O_3纳米纤维/Ce_(0.9)Gd_(0.1)O_2纳米粒子复合材料的合成与表征

5. Sonochemical synthesis and characterization of cobalt doped iron oxide nanoparticles, and immobilization of enzymes on gamma-iron oxide nanoparticles. [D] . Dyal, Ansil S. 2005

机译：声化学法合成和表征钴掺杂的氧化铁纳米颗粒，以及将酶固定在γ-氧化铁纳米颗粒上。

6. Synthesis and Characterization of Amorphous Iron Oxide Nanoparticles by the Sonochemical Method and Their Application for the Remediation of Heavy Metals from Wastewater [O] . Virendra Kumar Yadav, Daoud Ali, Samreen Heena Khan, 2020

机译：多晶硅法的合成与表征多晶硅氧化物纳米粒子及其在废水中重金属修复的应用

7. Synthesis and Characterization of Novel Zr-Al2O3 Nanoparticles Prepared by Microemulsion Method and Its Use as Cobalt Catalyst Support for the CO Hydrogenation Reaction [O] . Fatima Pardo-Tarifa, Saul Cabrera, Margarita Sanchez-Dominguez, 2017

机译：通过微乳液法制备的新型Zr-Al2O3纳米粒子的合成与表征及其用作氢化反应的钴催化剂载体

1. C20分子与C20-、C202-离子的特性分析与比较 [J] . 张秀梅 ,王利光 ,王志萍 . 原子与分子物理学报 . 2012,第001期

2. 人红细胞20S蛋白酶体的蛋白质组学表征及不同来源20S蛋白酶体异质性的研究 [J] . 陈国强 ,刘辉 ,张海婧 . 分析化学 . 2009,第012期

3. 在第二届海峡论坛大会上的致辞（20o年6月20日） [J] . 王毅 . 两岸关系 . 2012,第006期

4. 服用三七后人尿液中20（S）-原人参三醇及其20S，24S-环氧化物的定性定量分析 [J] . 赵宇新 . 国外医学：中医中药分册 . 2003,第005期

5. 337 服用三七后人尿液中20(S)-原人参三醇及其20S,24S-环氧化物的定性定量分析 [J] . . 国际中医中药杂志 . 2003,第005期

6. 低热中子吸收截面Al20Mo20Nb20V20Zr20高熵合金涂层的制备及表征 [C] . ZHANG Wei ,张伟 ,YANG Ji-jun . 中国核学会2023年学术年会 . 2017

7. （20S）-20-羟基胆甾烷-3，16-二酮的首次合成 [A] . 唐仕阳 . 2007

1. 合成司班－20、司盘－20或失水山梨醇单月桂酸酯表面活性剂的生产工艺 [P] . 中国专利： CN1250683A . 2000-04-19

2. 20(R)-25-羟基-达玛烷型-3β,12β,20-三醇的药物用途 [P] . 中国专利： CN111228277A . 2020-06-05

3. METHOD FOR LIQUID-PHASE SYNTHESIS OF MULTI-COMPONENT CERAMIC MATERIAL IN ZrO₂-Y₂O₃-Gd₂O₃-MgO SYSTEM FOR PRODUCTION OF ELECTROLYTE FOR SOLID OXIDE FUEL CELL [P] . 外国专利： RU2614322C1 . 2017-03-24

机译：ZrO _{2 -Y _{2 O _{3 -Gd _{2 O _{3 -MgO系统生产固体氧化物燃料电池用电解质}}}}}

4. USE OF ARYL OXIDES OF ISOBUTYL ALUMINIUM AS ACTIVATORS DIALKYL METALLOCENE CATALYSTS FOR HOMOPOLYMERISATION ETHYLENE, PROPYLENE, COPOLYMERISATION OF ETHYLENE WITH PROPYLENE AND TRIPLE COPOLYMERISATION OF ETHYLENE, PROPYLENE AND DIENE, HOMOGENEOUS METALLOCENE CATALYST SYSTEMS FOR SYNTHESIS OF HOMO-AND COPOLYMERS OF OLEFINS AND DIENES, METHOD OF PRODUCING HOMO- AND COPOLYMERS OF OLEFINS AND DIENES, METHOD FOR STABILISATION OF HOMO- AND COPOLYMERS OF OLEFINS AND DIENES [P] . 外国专利： RU0002588496C2 . 2016-06-27

机译：异丁基铝的芳烃氧化物作为二烷基金属茂催化剂的活化剂，用于均聚乙烯，丙烯，乙烯与丙烯的共聚以及乙烯，丙烯和二烯的三元共聚，丙烯和二烯，乙烯和二烯生产烯烃和二烯的均聚物和共聚物，稳定烯烃和二烯的均聚物和共聚物的方法

5. METHOD FOR PREPARING SILVER OXIDE USING CATHODIC ELECTROCHEMICAL SYNTHESIS AND SILVER OXIDE NANOPARTICLES PREPARED THEREBY [P] . 外国专利： KR101650084B1 . 2016-08-22

机译：阴极电化学合成制备氧化银的方法及由此制备的氧化银纳米粒子

相关主题

Synthesis and characterization of Gd2Zr2O7 defect-fluorite oxide nanoparticles via a homogeneous precipitation-solvothermal method

摘要

著录项

相似文献

相关主题

期刊订阅

Synthesis and characterization of Gd₂Zr₂O₇ defect-fluorite oxide nanoparticles via a homogeneous precipitation-solvothermal method