Synthesis and characterization of Gd2Zr2O7 defect-fluorite oxide nanoparticles via a homogeneous precipitation-solvothermal method

Tang Zhe; Huang Zhangyi; Qi Jianqi; Guo Xiaofeng; Han Wei; Zhou Mao; Peng Shuting; Lu Tiecheng

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Synthesis and characterization of Gd2Zr2O7 defect-fluorite oxide nanoparticles via a homogeneous precipitation-solvothermal method

机译：Gd2Zr2O7缺陷 - 氟盐氧化物纳米粒子通过均相沉淀 - 溶剂溶液的合成与表征

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Defect-fluorite structured Gd2Zr2O7 nanoparticles were successfully synthesized via a homogeneous precipitation-solvothermal method using urea as a precipitant. The obtained nanoparticles were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), Brunauer-Emmett-Teller (BET) analysis and transmission electron microscopy (TEM). Compared to the traditional solvothermal method, this homogeneous precipitation-solvothermal method has the advantage of producing nanoparticles with small grain sizes, a narrow sizedistribution, high surface areas and little agglomeration. Particularly, the mean crystallite size of Gd2Zr2O7 obtained by this method is 20-30 nm, providing a great opportunity of using these nanoparticles as starting nano-sized building blocks for low temperature preparation of homogeneous and dense ceramics.

机译：使用尿素作为沉淀剂，通过均匀沉淀 - 溶剂的方法成功地合成缺陷萤石结构Gd2ZR2O7纳米颗粒。通过X射线衍射（XRD），傅里叶变换红外光谱（FT-IR），扫描电子显微镜（SEM），Brunauer-Emmett-Teller（BET）分析和透射电子显微镜（TEM）的所得纳米颗粒。与传统的溶剂热法相比，这种均匀的沉淀 - 溶剂热法具有生产具有小晶粒尺寸的纳米颗粒，狭窄的大小写，高表面积和少量集聚的优点。特别地，通过该方法获得的Gd2zR2O7的平均微晶尺寸为20-30nm，提供了使用这些纳米颗粒作为起始纳米大小构建块的机会，用于低温制备均匀和致密陶瓷。

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《RSC Advances》 |2017年第87期|共6页
作者
Tang Zhe; Huang Zhangyi; Qi Jianqi; Guo Xiaofeng; Han Wei; Zhou Mao; Peng Shuting; Lu Tiecheng;
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作者单位

Sichuan Univ Coll Phys Sci &

Technol Chengdu 610064 Sichuan Peoples R China;

Sichuan Univ Coll Phys Sci &

Technol Chengdu 610064 Sichuan Peoples R China;

Sichuan Univ Coll Phys Sci &

Technol Chengdu 610064 Sichuan Peoples R China;

Washington State Univ Dept Chem Pullman WA 99163 USA;

Sichuan Univ Coll Phys Sci &

Technol Chengdu 610064 Sichuan Peoples R China;

Sichuan Univ Coll Phys Sci &

Technol Chengdu 610064 Sichuan Peoples R China;

Sichuan Univ Coll Phys Sci &

Technol Chengdu 610064 Sichuan Peoples R China;

Sichuan Univ Coll Phys Sci &

Technol Chengdu 610064 Sichuan Peoples R China;

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正文语种 eng
中图分类化学;
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1. Synthesis and characterization of Gd2Zr2O7 defect-fluorite oxide nanoparticles via a homogeneous precipitation-solvothermal method [J] . Tang Zhe, Huang Zhangyi, Qi Jianqi, RSC Advances . 2017,第87期

机译：Gd2Zr2O7缺陷 - 氟盐氧化物纳米粒子通过均相沉淀 - 溶剂溶液的合成与表征
2. Synthesis, Characterization and Anti-Microbial Activity of Oxalate-Assisted CO3O4 Nanoparticles Derived from Homogeneous Co-Precipitation Method [J] . C. T. Anuradha, P. Raji International journal of nanoscience . 2019,第5期

机译：均相共沉淀法衍生的草酸盐辅助CO3O4纳米颗粒的合成，表征及抗微生物活性
3. Synthesis of Co3O4-ZnO mixed metal oxide nanoparticles by homogeneous precipitation method [J] . Sharma Ravi Kant, Ghose Ranjana Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics . 2016,第Null期

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4. Preparation and Characterization of Gd2Zr2O7 Nanoparticles via the Citric Acid Chelating Agent Method [C] . Lei Ma, Weimin Ma, Xudong Sun International conference on Testing and Evaluation of Inorganic Materials . 2013

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Synthesis and characterization of Gd2Zr2O7 defect-fluorite oxide nanoparticles via a homogeneous precipitation-solvothermal method

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