Influence of the substituent D/A at the 1,2,3-triazole ring on novel terpyridine derivatives: synthesis and properties

Dawid Zych; Aneta Slodek; D?astin Zimny; Sylwia Golba; Katarzyna Malarz; Anna Mrozek-Wilczkiewicz

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Influence of the substituent D/A at the 1,2,3-triazole ring on novel terpyridine derivatives: synthesis and properties

机译：1,2,3-三唑环上的取代基D / A对新型联吡啶衍生物的影响：合成与性能

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In this study, we newly designed and developed a synthesis route based on the 1,3-dipolar cycloaddition of the derivatives of 4′-(1,2,3-triazol-4-yl)phenyl-2,2′:6′,2′′-terpyridine with various (hetero)aryl substituents, differing in electronic character, on a triazol ring. The obtained compounds were comprehensively characterized by UV-Vis spectroscopy and electrochemical and thermal studies. Moreover, preliminary biological tests were conducted. The investigation allowed the selection of materials with the most promising properties with particular emphasis on the nature of the substituents. In addition, theoretical studies (DFT and TD-DFT) were performed to verify the comprehensive understanding of experimental results.

机译：在这项研究中，我们根据4'-（1,2,3-三唑-4-基）苯基-2,2'：6'的衍生物的1,3-偶极环加成反应设计并开发了一种合成路线在三唑环上具有各种电子特性不同的（杂）芳基取代基的2，'-叔吡啶。通过紫外-可见光谱以及电化学和热学研究对获得的化合物进行了全面表征。此外，进行了初步的生物学测试。研究允许选择具有最有希望的性能的材料，特别强调取代基的性质。此外，进行了理论研究（DFT和TD-DFT）以验证对实验结果的全面理解。

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《RSC Advances》 |2019年第29期|共11页
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Dawid Zych; Aneta Slodek; D?astin Zimny; Sylwia Golba; Katarzyna Malarz; Anna Mrozek-Wilczkiewicz;
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1. Influence of the substituent D/A at the 1,2,3-triazole ring on novel terpyridine derivatives: synthesis and properties [J] . Zych Dawid, Slodek Aneta, Zimny Dzastin, RSC Advances . 2019,第29期

机译：取代基D / A对新型三吡啶衍生物1,2,3-三唑环的影响：合成与性能
2. Synthesis, crystal structures of a series of novel 2, 2 ':6 ', 2 ''-terpyridine derivatives: The influences of substituents on their photophysical properties and intracellular acid organelle targeting [J] . Liu Jie, Zhu Yingzhong, Tian Xiaohe, Dyes and Pigments . 2016,第Null期

机译：一系列新颖的2、2'：6'，2''-吡啶吡啶衍生物的合成，晶体结构：取代基对其光物理性质和细胞内酸性细胞器靶向的影响
3. Synthesis and antimicrobial of some new substituted tetrazolomethylbenzo[d]-[1,2,3]triazole derivatives using 1H-benzo[d][1,2,3]triazole as starting material [J] . Omar M. Ali, Abd El-Galil E. Amr, Elsayed E. Mostafa Research on Chemical Intermediates . 2014,第4期

机译：以1H-苯并[d] [1,2,3]三唑为起始原料合成某些新的取代的四唑甲基苯并[d]-[1,2,3]三唑衍生物及其抗菌性能
4. Synthesis, single crystal structure and performance of N-Arylsubstituted of 1,2,3-triazole derivatives [C] . Yan-yang QU, Xin HUANG, Jun WANG, International conference on defence technology;China Ordnance Society . 2018

机译：1,2,3-三唑衍生物的N-芳基取代基的合成，单晶结构和性能
5. Synthesis of evaluation of beta-glycosyl-1,2,3-triazole derivatives as beta-glycosidase inhibitors. [D] . Rossi, Lauren Lucille. 2007

机译：合成评价β-糖基-1,2,3-三唑衍生物作为β-糖苷酶抑制剂。
6. Synthesis and Biological Properties of Novel Triazole-Thiol and Thiadiazole Derivatives of the 124-Triazole-3(5)-one Class [O] . Esra Düğdü, Yasemin Ünver, Dilek Ünlüer, 2014

机译：124-三唑-3（5）-一类新型三唑-硫醇和噻二唑衍生物的合成及生物学性质
7. Influence of the substituent D/A at the 1,2,3-triazole ring on novel terpyridine derivatives: synthesis and properties [O] . Dawid Zych, Aneta Slodek, Dżastin Zimny, 2019

机译：取代基D / A对新型三吡啶衍生物1,2,3-三唑环的影响：合成与性能
8. The Crystal and Molecular Structure of 2-Phenyl-4,5-Dianilino-2H-1,2,3-Triazole; Correlation between the Asymmetry of the Triazole Ring and the Conformations of the Anilino Substituents [R] . Harlow, R. L., Brown, S. B., Dewar, M. J. S., 1976

机译：2-苯基-4,5-二苯胺基-2H-1,2,3-三唑的晶体和分子结构;三唑环的不对称性与苯胺基取代基构象的相关性

Influence of the substituent D/A at the 1,2,3-triazole ring on novel terpyridine derivatives: synthesis and properties

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