FeF3-catalyzed MCR in PEG-400: ultrasound assisted synthesis of N-substituted 2-aminopyridines

Dinne Naresh Kumar Reddy; Kothapalli Bannoth Chandrasekhar; Yaddanapudi Sesha Siva Ganesh; G. Rajeshwar Reddy; J. Pradeep Kumar; Ravi Kumar Kapavarapu; Manojit Pal

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FeF3-catalyzed MCR in PEG-400: ultrasound assisted synthesis of N-substituted 2-aminopyridines

机译：PEG-400中的FEF3催化MCR：超声辅助合成N取代的2-氨基吡啶

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FeF _(3) catalyzed four component reaction under ultrasound irradiation was explored for the first time to prepare N -substituted 2-aminopyridines in good yields. The methodology involved the use of readily available starting materials and PEG-400 under mild reaction conditions in the presence of air. The one-pot methodology afforded a range of compounds of pharmacological interest indicating its potential in generating a diversity based library of small molecules useful for medicinal chemistry and drug discovery.

机译：FEF _（3）首次探讨了超声辐射下的四种组分反应，以良好的产率制备N-仲丁的2-氨基吡啶。该方法涉及在空气存在下在温和的反应条件下使用容易获得的起始材料和PEG-400。单壶方法理提供了一系列药理兴趣的化合物，表明其在产生一种可用于药物化学和药物发现的小分子的基于分子的潜力。

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《RSC Advances》 |2016年第71期|共6页
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Dinne Naresh Kumar Reddy; Kothapalli Bannoth Chandrasekhar; Yaddanapudi Sesha Siva Ganesh; G. Rajeshwar Reddy; J. Pradeep Kumar; Ravi Kumar Kapavarapu; Manojit Pal;
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1. FeF3-catalyzed MCR in PEG-400: ultrasound assisted synthesis of N-substituted 2-aminopyridines [J] . Reddy Dinne Naresh Kumar, Chandrasekhar Kothapalli Bannoth, Ganesh Yaddanapudi Sesha Siva, RSC Advances . 2016,第71期

机译：PEG-400中的FEF3催化MCR：超声辅助合成N取代的2-氨基吡啶
2. An efficient and chemoselective synthesis of N-substituted 2-aminopyridines via a microwave-assisted multicomponent reaction [J] . Shujiang Tu, Bo Jiang, Yan Zhang, Organic & biomolecular chemistry . 2007,第2期

机译：通过微波辅助的多组分反应高效且化学选择性地合成N-取代的2-氨基吡啶
3. Ultrasound-assisted green one-pot synthesis of linked bis-heterocycle peptidomimetics via IMCR/post-transformation/tandem strategy [J] . Kaveti Bhavna, Ramirez-Lopez Sandra C., Gamez Montano Rocio Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2018,第49期

机译：通过IMCR /后转换/串联策略通过IMCR /串联策略进行超声辅助绿色一锅合成链接的双杂杂蛋白肽模拟物
4. Synthesis and X-ray Structural Studies Of Novel Metal-Organic Complex: Diiodobis(2-aminopyridine)Cadmium(II) Single Crystal [C] . Venkatesan. G, Anandha Babu. G, Ramasamy. P DAE Solid State Physics Symposium . 2014

机译：新型金属 - 有机复合物的合成与X射线结构研究：二碘缺鼠（2-氨基吡啶）镉（II）单晶
5. I. Studies towards the total synthesis of (+/-)-lycoramine. II. Development of the retro-aza-Claisen rearrangement to synthesize medium sized N-substituted heterocycles. III. Studies towards the total synthesis of (-)-nakadomarin A. [D] . Genung, Nathan Edward. 2009

机译：I.关于（+/-）-lycoramine的全合成的研究。二。反氮-克莱森重排的发展，以合成中等大小的N-取代的杂环。三，对（-）-nakadomarin A的全合成的研究。
6. N-Substituted 5-Amino-6-methylpyrazine-23-dicarbonitriles: Microwave-Assisted Synthesis and Biological Properties [O] . Ondrej Jandourek, Martin Dolezal, Pavla Paterova, 2014

机译：N取代的5-氨基-6-甲基吡嗪-23-二腈：微波辅助合成及生物学性质
7. Ultrasound assisted multicomponent reactions: A green method for the synthesis of N-substituted 1,8-dioxo-decahydroacridines using β-cyclodextrin as a supramolecular reusable catalyst in water [O] . Asha V. Chate, Umesh B. Rathod, Jagdish S. Kshirsagar, 2016

机译：超声辅助多组分反应：使用β-环糊精为基于水中的β-环糊精的N-取代的1,8-二氧基 - 甲基吖啶吖啶吖啶的绿色方法作为水中的超分子可再用催化剂

FeF3-catalyzed MCR in PEG-400: ultrasound assisted synthesis of N-substituted 2-aminopyridines

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