Validation of a multi residue SBSE-RTL-GC-MS method for the quantitative analysis of 54 pesticide residues in fruit and vegetables

B. Klaubert; H. Tomfoerde; K. Schad

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Validation of a multi residue SBSE-RTL-GC-MS method for the quantitative analysis of 54 pesticide residues in fruit and vegetables

机译：验证多残留SBSE-RTL-GC-MS方法对水果和蔬菜中54种农药残留进行定量分析的有效性

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For the determination of pesticide residues in fruit and vegetables various analytical methods are available. Besides the reference procedures EN 12393/DFGS19 for the gas chromatographic analysis of pesticides, the fast and cheap QuEChERS-technique is one of the most popular extraction procedures for the analysis of residues by GC-MS and LC-MS [1]. Anyhow solvent free extraction techniques display also an essential role in sample clean-up. After introduction of the solid-phase mic-roextraction (SPME) by J. Pawliszyn in the early nineties, stir bar sorptive extraction (SBSE) in combination with thermode-sorption and automated retention-time-locking GC-MS (RTL-GC-MS) became an interesting alternative for residue screening in fruit and vegetables.

机译：为了测定水果和蔬菜中的农药残留，可以使用各种分析方法。除了用于农药气相色谱分析的参考程序EN 12393 / DFGS19之外，快速而廉价的QuEChERS技术是通过GC-MS和LC-MS分析残留物的最受欢迎的萃取程序之一[1]。无论如何，无溶剂萃取技术在样品净化中也显示出至关重要的作用。在90年代初期，J。Pawliszyn引入了固相微萃取（SPME）后，搅拌棒吸附萃取（SBSE）与热脱附和自动保留时间锁定GC-MS（RTL-GC- MS）成为水果和蔬菜中残留物筛查的有趣替代方法。

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《Lebensmittelchemie》 |2008年第4期|p.95-96|共2页
作者
B. Klaubert; H. Tomfoerde; K. Schad;
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Central Institute of the Bundeswehr Medical Service Munich, Garching-Hoch-brueck;

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正文语种 eng
中图分类食品工业;
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1. A novel optimised and validated method for analysis of multi-residues of pesticides in fruits and vegetables by microwave-assisted extraction (MAE)-dispersive solid-phase extraction (d-SPE)-retention time locked (RTL)-gas chromatography-mass spectrometry with Deconvolution reporting software (DRS) [J] . Gouri Satpathy, Yogesh Kumar Tyagi, Rajinder Kumar Gupta Food Chemistry . 2011,第3期

机译：微波辅助萃取（MAE）-分散固相萃取（d-SPE）-保留时间锁定（RTL）-气相色谱-质谱联用分析水果和蔬菜中多种农药残留的优化方法使用反卷积报告软件（DRS）
2. Development and validation of a multiresidue method for the determination of neonicotinoid and macrocyclic lactone pesticide residues in milk, fruits, and vegetables by ultra-performance liquid chromatography/MS/MS. [J] . Kamel A., Yaorong Qian, Kolbe E., Journal of AOAC International . 2010,第2期

机译：开发和验证一种通过超高效液相色谱/ MS / MS测定牛奶，水果和蔬菜中新烟碱和大环内酯农药残留的多残留方法。
3. Development and validation of a multi-residue method for the determination of pesticides in processed fruits and vegetables using liquid chromatography-electrospray ionization tandem mass spectrometry [J] . Botitsi H, Econornou A, Tsipi D Analytical and bioanalytical chemistry . 2007,第6期

机译：液相色谱-电喷雾串联质谱法测定水果和蔬菜中农药的多残留方法的建立和验证
4. Comparing GC/MS/MS to GC/MS Methods for the Analysis of Pesticide Residues in Fruits and Vegetables [C] . Philip L. Wylie, Chin-Kai Meng American Society for Mass Spectrometry Conference on Mass Spectrometry and Allied Topics . 2009

机译：将GC / MS / MS与GC / MS方法进行比较，用于分析水果和蔬菜中的农药残留物
5. Pesticide residues in imported frozen fruits and vegetables (Frozen foods). [D] . Ku, Katherine Oi Ming. 2000

机译：进口冷冻水果和蔬菜（冷冻食品）中的农药残留。
6. Overall and class-specific scores of pesticide residues from fruits and vegetables as a tool to rank intake of pesticide residues in United States: a validation study [O] . Yang Hu, Yu Han Chiu, Russ Hauser, -1

机译：水果和蔬菜中农药残留的总体和特定类别得分作为对美国农药残留摄入量进行排名的工具：一项验证研究
7. Validation Study on a Multi-Residue Method for Determination of Pesticide Residues in Vegetables and Fruits by using General Matrix Standard Solutions [O] . Naoki FUKUI, Satoshi TAKATORI, Satoko YAMAGUCHI, 2015

机译：一种多残留方法的验证研究通过使用通用基质标准溶液测定蔬菜和水果中的农药残留量

Validation of a multi residue SBSE-RTL-GC-MS method for the quantitative analysis of 54 pesticide residues in fruit and vegetables

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