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PRODUCTION OF ACTIVATED CARBON FROM RICE HUSK TO SUPPORT Zn2+ IONS

机译:从稻壳生产活性炭以支持Zn2 +离子

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摘要

The aim of this study is producing the low-cost activated carbon rice husks by chemical activation using zinc chloride (ZnCl2) at 700 degrees C in N-2 atmosphere. Impregnation ratios of 1:1 2:1 3:1 and 4:1 (g ZnCl2/g rice husk) have been used. The highest yield is obtained with the ratio of 4:1 and found 40.90. Zinc ions in the form of ZnNO3 have been added to the obtained product which has a higher pore size than the raw material. Obtained activated carbon and the ZnNO3 added products have then been characterized using Scanning electron microscopy (SEM) photos, X-ray diffractometer (XRD), Brunauer-Emmett-Teller (BET) surface analysis and Fourier transform infrared spectra (FTIR) methods. The BET surface area of the highest yield activated carbon has found 922.319 m(2/)g according to the results of the analysis. The results of this study will be useful in developing resource recovery systems for agricultural biomass. Results have that carbonization impregnation ratio have significant effect on the surface area and pore structure of the prepared activated carbon. The whole process can be summarized in the following steps; activation of the rice husk, carbonization, washing, preparing the RHC/Zn mixtures and characterization.
机译:这项研究的目的是通过在N-2气氛中在700摄氏度下使用氯化锌(ZnCl2)进行化学活化来生产低成本的活性炭稻壳。浸渍比为1:1 2:1 3:1和4:1(g ZnCl2 / g稻壳)。比例为4:1时,收率最高,为40.90。将ZnNO 3形式的锌离子添加到所获得的产物中,该产物具有比原料更大的孔径。然后使用扫描电子显微镜(SEM)照片,X射线衍射仪(XRD),Brunauer-Emmett-Teller(BET)表面分析和傅里叶变换红外光谱(FTIR)方法对获得的活性炭和ZnNO3添加产物进行表征。根据分析结果,活性炭产率最高的BET表面积为922.319 m(2 /)g。这项研究的结果将有助于开发农业生物质资源回收系统。结果表明,碳化浸渍率对制备的活性炭的表面积和孔结构具有显着影响。整个过程可以归纳为以下步骤:活化稻壳,碳化,洗涤,制备RHC / Zn混合物并进行表征。

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