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Proposal of Simplified Modified Williamson-Hall Equation

机译:简化的改进的Williamson-Hall方程的建议

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Williamson-Hall (WH) plots are characterized by irregular arrangement of data due to the elastic anisotropy in each {hkl} plane. In order to correct the effect of elastic anisotropy, Ungar developed a unique methodology using the contrast factor C, so called the modified Williamson-Hall (mWH) method. When X-ray with the wave length λ was used for diffraction analysis and diffraction angle 6 and integral breadth βt was obtained in each diffraction peak, the following mWH equation is constructed as functions of the parameter K (=2sinθ/λ) and ∆K (=βcosθ/λ). ∆K =α+φk√C+OK~2C Here, the parameter α is dependent on the crystallite size. The parameter φ and O are constants but the O-value is much smaller than the φ-value. In the mWH plots in 60% cold rolled ferrite (Fe-0.0056%C), ultra low carbon martensite (Fe-18%Ni) and 20% cold rolled austenite (SUS316L), it was confirmed that the value of OK~2C is negligibly small. As a result, the following simplified equation is applicable for the analysis by mWH method. ∆K =α+φk√C
机译:由于每个{hkl}平面中的弹性各向异性,Williamson-Hall(WH)图的特征在于数据的不规则排列。为了校正弹性各向异性的影响,Ungar开发了一种使用对比度因子C的独特方法,即所谓的改进的Williamson-Hall(mWH)方法。当使用波长为λ的X射线进行衍射分析并在每个衍射峰中获得衍射角6和积分宽度βt时,以下mWH方程将作为参数K(=2sinθ/λ)和∆K的函数构建(=βcosθ/λ)。 ΔK=α+φk√C+ OK〜2C在此,参数α取决于微晶尺寸。参数φ和O是常数,但是O值比φ值小得多。在60%冷轧铁素体(Fe-0.0056%C),超低碳马氏体(Fe-18%Ni)和20%冷轧奥氏体(SUS316L)的mWH图中,确定OK〜2C的值为小到可以忽略不计。结果,以下简化方程适用于通过mWH方法进行的分析。 ΔK=α+φk√C

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