Large-scale synthesis of (Bi(Bi_2S_3)_9I_3)_(0.667) submicrometer needle-like crystals via a novel polyol route

Guozhen Shen; Di Chen; Kaibin Tang; Liying Huang; Yitai Qian

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Large-scale synthesis of (Bi(Bi_2S_3)_9I_3)_(0.667) submicrometer needle-like crystals via a novel polyol route

机译：通过新型多元醇途径大规模合成（Bi（Bi_2S_3）_9I_3）_（0.667）亚微米针状晶体

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摘要

Needle-like (Bi(Bi_2S_3)_9I_3)_(0.667) crystals have been synthesized by a polyol method at 195℃ for the first time. X-ray diffraction pattern, scanning electron microscopy and transmission electron microscopy were used to characterize the product, which revealed that the product consisted of needle-like crystals about 400 nm in diameter and length up to 15 μm and the possible formation mechanism was also discussed.

机译：首次在195℃下通过多元醇法合成了针状（Bi（Bi_2S_3）_9I_3）_（0.667）晶体。用X射线衍射图谱，扫描电镜和透射电镜对产物进行表征，结果表明产物由直径约400 nm，长度达15μm的针状晶体组成，并讨论了可能的形成机理。。

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来源
《Journal of Crystal Growth》 |2003年第2期|p.331-334|共4页
作者
Guozhen Shen; Di Chen; Kaibin Tang; Liying Huang; Yitai Qian;
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作者单位

Department of Chemistry and Structure Research Laboratory, University of Science and Technology of China, Hefei 230026, People's Republic of China;

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收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
原文格式 PDF
正文语种 eng
中图分类晶体学;
关键词
A1. low dimensional structures; A2. growth from solutions; B1. bismuth compounds;

机译：A1。低维结构;A2。解决方案的增长;B1。铋化合物;

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Large-scale synthesis of (Bi(Bi_2S_3)_9I_3)_(0.667) submicrometer needle-like crystals via a novel polyol route

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