Synthesis, Characterization of α-Oxopentanedioic Acid-Isonicotinoyl Hydrazone Rare Earth- Complexes and Relaxivity of Gd- complex

Yang Zhengyin; Yang Rudong

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Synthesis, Characterization of α-Oxopentanedioic Acid-Isonicotinoyl Hydrazone Rare Earth- Complexes and Relaxivity of Gd- complex

机译：α-氧杂戊二酸-异烟酰ylyl稀土配合物的合成，表征及Gd配合物的弛豫性

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α-Oxopentanedioic acid isonicotinoyl hydrazone (H_2L) and its five rare earth complexes were synthesized with a view to further investigating MRI activities of the polycarboxylic Schiff base complexes. The complexes were characterized on the basis of elemental analyses, IR, UV, ~1H NMR spectra and thermal analyses. The general formula of the complexes is [Ln(HL)(H_2O)_2]Cl_2·H_2O (where Ln(Ⅲ) = La, Pr, Nd, Eu and Gd). In addition, the relaxivity (R_1) of the Gd-complex was determined by INVREC Au program.

机译：为了进一步研究聚羧酸席夫碱配合物的MRI活性，合成了α-氧戊二烯酸异烟酰ino（H_2L）及其5种稀土配合物。根据元素分析，IR，UV，〜1H NMR光谱和热分析对络合物进行表征。配合物的通式为[Ln（HL）（H_2O）_2] Cl_2·H_2O（其中Ln（Ⅲ）= La，Pr，Nd，Eu和Gd）。另外，通过INVREC Au程序确定Gd复合物的弛豫度（R_1）。

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《Journal of rare earths》 |2004年第3期|p.327-330|共4页
作者
Yang Zhengyin; Yang Rudong;
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正文语种 eng
中图分类工业经济理论;化学;
关键词
inorgonic chemistry; MRI contrast agent; relaxivity; rare earth complexes;

机译：无机化学;MRI造影剂;松弛度;稀土配合物;

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1. Synthesis, Characterization of α-Oxopentanedioic Acid-Isonicotinoyl Hydrazone Rare Earth- Complexes and Relaxivity of Gd- complex [J] . Yang Zhengyin, Yang Rudong Journal of rare earths . 2004,第3期

机译：α-氧戊二烯酸-异烟酰yl Hy稀土配合物的合成，表征及Gd配合物的弛豫性
2. Synthesis and relaxivity of polycarboxylic hydrazone rare earth complexes -Relaxivity of α-oxo-pentanedioic acid benzoyl hydrazone Gd-complexes [J] . YANG Zhengyin, LI Fashen, YANG Li Chinese science bulletin . 2000,第20期

机译：多元羧酸稀土配合物的合成与弛豫度-α-氧代戊二酸苯甲酰Gd配合物的弛豫性
3. Rare Earth Complexes with 3-Carbaldehyde Chromone-(Benzoyl) Hydrazone: Synthesis, Characterization, DNA Binding Studies and Antioxidant Activity [J] . Li Y, Yang ZY Journal of Fluorescence . 2010,第1期

机译：稀土与3-甲醛苯并（苯甲酰基）dra的配合物：合成，表征，DNA结合研究和抗氧化活性
4. Synthesis, Characterization of Polycarboxylic Isonicotinoyl Hydrazone Rare Earth Complexes (Ⅰ) [C] . International symposium on solid state chemistry in China amp; 8th Chinese national conference on solid state chemistry and inorganic synthesis : Book of abstracts . 2002

机译：聚羧酸异烟酰yl Hy稀土配合物的合成，表征（Ⅰ）
5. Studies of novel synthesis of functionalized polycyclic ring systems through the coupling reactions of Fischer carbene chromium complexes with enyne hydrazones and aldehydes. [D] . Ranchigoda Gamage, Lalith Santha. 2013

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机译：具有新型席夫碱Hy的Cu（II），Co（II），Mn（II），Fe（II）和UO2（VI）配合物的合成，表征和生物活性：O-羟基乙酰苯-7-chloro-4-喹Hy Hy

Synthesis, Characterization of α-Oxopentanedioic Acid-Isonicotinoyl Hydrazone Rare Earth- Complexes and Relaxivity of Gd- complex

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