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Aging characteristics and properties of Fe-16Cr-2.5Mo-1.0Cu damping alloy

机译:Fe-16Cr-2.5Mo-1.0Cu阻尼合金的时效特性和性能

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The precipitating behavior of Cu-riched particles during isothermally aging and its effect on hardness and damping capacity of Fe-16Cr-2.5Mo-1.0Cu damping alloy have been investigated by atom probe tomography (APT) and scanning transmission electron microscopy (STEM). The results show that aging at temperature range from 400 °C to 700 °C has minor influence on grain size. During aging at temperature below 400 °C, the supersaturated Cu dose not precipitate out. While aging temperature is 450 °C, a relatively small number of Cu-riched particles can be observed and the particle radius is small (1.5 ± 0.56 nm). With a further increasing aging temperature, the Cu-riched particles increase to 3.21 ± 0.52 nm at 550 °C and further grow to 12.88 ± 2.02 nm at 700 °C. As compared with 450 °C, the particle number increases significantly at 550 °C, and then decreases at 700 °C. Due to the stable grain size and no precipitate, the hardness keeps constant below 400 °C. With a further increasing aging temperature, the hardness increases gradually and reaches peak value aging at 600 °C due to the increase of Cu-riched particle number. The damping capacity significantly depends on particle. Once there appear Cu-riched particles, the damping capacity decreases obviously. During aging, both hardness and damping capacity of the alloy can keep stable when temperature is below 400 °C.
机译:通过原子探针层析成像(APT)和扫描透射电子显微镜(STEM)研究了富铜颗粒在等温时效过程中的析出行为及其对Fe-16Cr-2.5Mo-1.0Cu阻尼合金的硬度和阻尼性能的影响。结果表明,在400 C至700 C的温度范围内时效对晶粒尺寸的影响较小。在低于400 C的温度下老化期间,过饱和的Cu不会沉淀出来。时效温度为450 C时,可以观察到少量的富Cu粒子,且粒子半径较小(1.5±0.56 nm)。随着老化温度的进一步升高,富铜颗粒在550°C时增加到3.21±0.52nm,在700°C时进一步生长到12.88±2.02nm。与450°C相比,颗粒数在550°C下显着增加,然后在700°C下下降。由于晶粒尺寸稳定且无沉淀,因此硬度在400 C以下保持恒定。随着时效温度的进一步升高,由于富Cu颗粒数量的增加,硬度逐渐增加,并在600 C达到峰值时效。阻尼能力明显取决于颗粒。一旦出现富铜颗粒,阻尼能力明显下降。在时效过程中,温度低于400 C时,合金的硬度和阻尼能力都可以保持稳定。

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