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Study on the thermal and mechanical properties of novel neutron shielding composite laminates at elevated temperature

机译:新型中子屏蔽复合层合物在高温下的热力学性能研究

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摘要

Neutron shielding fibre metal laminates (NSFMLs) containing 10-50 wt% of boron carbide (B_4C) powder were fabricated using hot molding process, and the effects of experimental temperature on the thermal and mechanical properties of composite laminates were investigated in this work. Thermal stability of composite laminates was conducted with thermo-gravimetric analysis (TGA) and differential scanning calorimetry (DSC), and their mechanical properties were also measured. The testing results indicated that good interfacial adhesion between different layers, uniform distribution of B_4C particles and carbon fibres tightly surrounded by polyimide (PI) resin were crucial to the mechanical properties of composite laminates. TGA-DSC results illustrated the scarcely mass loss of composite laminates below 300 ℃, yet began to decompose when it exceeded over 390 ℃. Moreover, tensile strength of the NSFMLs degraded with the increasing of experimental temperature and the volume fraction of B_4C powder. Double bear shear (DBS) testing results showed that the NSFMLs with 30 wt% of B_4C powder had the maximum interlaminar shear value, while the primary delamination zone occurred at the interface between two layered carbon fibre reinforced prepregs (CFRPs). The composite laminates still maintained the good interlaminar shear strength even at 300 ℃.
机译:采用热成型工艺制备了含10-50 wt%碳化硼(B_4C)粉末的中子屏蔽纤维金属层压板(NSFML),并研究了实验温度对复合层压板热力学性能的影响。用热重分析(TGA)和差示扫描量热法(DSC)进行复合材料层压板的热稳定性,并测量其机械性能。测试结果表明,不同层之间的良好界面粘合性,B_4C颗粒的均匀分布以及被聚酰亚胺(PI)树脂紧密包围的碳纤维对复合材料层压板的机械性能至关重要。 TGA-DSC结果表明,复合层压板在300℃以下几乎没有质量损失,但在超过390℃时却开始分解。此外,随着实验温度和B_4C粉末体积分数的增加,NSFMLs的拉伸强度降低。双熊剪切(DBS)测试结果表明,含有30 wt%B_4C粉末的NSFML具有最大的层间剪切值,而主要的分层区域出现在两层碳纤维增强预浸料(CFRP)之间的界面上。即使在300℃时,复合层压板仍保持良好的层间剪切强度。

著录项

  • 来源
    《Materials Science and Engineering》 |2017年第14期|101-110|共10页
  • 作者单位

    College of Material Science & Technology, Nanjing University of Aeronautics & Astronautics, Nanjing 211106, China,Department of Mechanical & Electronic Engineering, Jiangsu Polytechnic of Finance & Economics, Huai'an, Jiangsu 223003, China,Jiangsu Collaborative Innovation Center for Advanced Inorganic Function Composites, Nanjing 211106, China;

    College of Material Science & Technology, Nanjing University of Aeronautics & Astronautics, Nanjing 211106, China,Jiangsu Collaborative Innovation Center for Advanced Inorganic Function Composites, Nanjing 211106, China;

    College of Material Science & Technology, Nanjing University of Aeronautics & Astronautics, Nanjing 211106, China,Jiangsu Collaborative Innovation Center for Advanced Inorganic Function Composites, Nanjing 211106, China;

    College of Material Science & Technology, Nanjing University of Aeronautics & Astronautics, Nanjing 211106, China,Jiangsu Collaborative Innovation Center for Advanced Inorganic Function Composites, Nanjing 211106, China;

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  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    Neutron shielding fibre metal laminates (NSFMLs); Thermal properties; Interlaminar shear (ILS) strength; Hot molding process;

    机译:中子屏蔽纤维金属层压板(NSFML);热性能;层间剪切(ILS)强度;热成型工艺;

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