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首页> 外文期刊>Materials Science and Engineering. A, Structural Materials >Fracture behaviour of thermal barrier coatings after high temperature exposure in air
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Fracture behaviour of thermal barrier coatings after high temperature exposure in air

机译:空气中高温暴露后隔热涂层的断裂行为

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摘要

Four point bending tests have been carried out on thermal barrier coating (TBC) specimens. The system studied consists of a plasma sprayed top coat (TC) of ZrO_2 6-8 wt.% Y_2O_3 (YSZ), an FeNiCrAlY bond coat (BC) and a mild steel substrate. To study the influence of temperature on this system, two heat treatments were adopted. The specimens were held in a furnace for 2 h at 580 and 900℃, and cooled inside the furnace to room temperature (RT). In addition, microstructural analyses were carried out after each treatment by using different techniques energy dispersive X-ray analysis (EDX); X-ray diffraction (XRD); Raman spectroscopy, and scanning electron microscopy (SEM)). Four point bending tests were carried out on heat-treated specimens and the results were compared with those for the as-sprayed condition. In situ observation of crack propagation events were carried out during the tests and it was found that cracks propagated through the TC-BC interface in specimens heat-treated at 580℃ heat treatment and also in the as-sprayed reference specimens. In contrast, after the 900℃ heat treatment they propagated across the BC-substrate interface. The drop in BC-substrate adhesion due to heat treatment at 900℃ prevailed over the mechanical weakness induced at the TC-BC interface.
机译:已经对热障涂层(TBC)样品进行了四点弯曲测试。所研究的系统由ZrO_2 6-8 wt。%Y_2O_3(YSZ)的等离子喷涂面涂层(TC),FeNiCrAlY粘结涂层(BC)和低碳钢基材组成。为了研究温度对该系统的影响,采用了两种热处理方法。将样品在580和900℃的炉子中放置2小时,然后在炉子内冷却至室温(RT)。另外,在每次处理之后,通过使用不同的技术能量色散X射线分析(EDX)进行了显微结构分析。 X射线衍射(XRD);拉曼光谱和扫描电子显微镜(SEM))。对热处理过的样品进行四点弯曲测试,并将结果与​​喷涂条件下的结果进行比较。在测试过程中对裂纹扩展事件进行了现场观察,发现在580℃热处理的试样以及喷涂的参考试样中,裂纹均通过TC-BC界面扩展。相反,在900℃热处理后,它们在BC-底物界面上传播。由于在900℃下进行热处理而导致的BC-基底粘附力下降超过了TC-BC界面引起的机械弱点。

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