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Microwave sintering of ZnO nanopowders and characterization for gas sensing

机译:ZnO纳米粉的微波烧结及其气敏特性

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摘要

Thick film gas sensors based on ZnO nanopowders were fabricated by using microwave sintering. The surface and cross section morphologies were characterized by field-emission scanning electron microscopy (FE-SEM). The stability of the microstructure was studied by impedance spectroscopy. The results showed that the shape of the nanoparticles was not changed through microwave sintering, and the thick films had the more dense microstructures than that by muffle oven sintering. The resistance-temperature characteristic and the responses to toluene, methanol and formaldehyde revealed that the microwave sintering technique could effectively control the growth of ZnO nanoparticles, realize the uniform sintering of thick film, gain the stable microstructure and improve the response of sensor. In addition, the formative mechanism of the thick film microstructure was proposed according to microwave sintering mechanism.
机译:通过微波烧结制备了基于ZnO纳米粉的厚膜气体传感器。通过场发射扫描电子显微镜(FE-SEM)表征表面和横截面的形态。通过阻抗光谱研究了微结构的稳定性。结果表明,通过微波烧结,纳米颗粒的形状没有改变,厚膜的组织比马弗炉烧结的致密。电阻-温度特性以及对甲苯,甲醇和甲醛的响应表明,微波烧结技术可以有效地控制ZnO纳米粒子的生长,实现厚膜的均匀烧结,获得稳定的微观结构,并改善传感器的响应。另外,根据微波烧结机理,提出了厚膜微结构的形成机理。

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  • 来源
    《Materials Science and Engineering》 |2011年第2期|p.181-186|共6页
  • 作者单位

    Key Lab for Green Processing and Functionalization of New Textile Materials, Ministry of Education, Wuhan Textile University, Wuhan 430073, PR China;

    State Key Laboratory of Material Processing and Die & Mould Technology, Huazhong University of Science and Technology, Wuhan 430074, PR China;

    State Key Laboratory of Material Processing and Die & Mould Technology, Huazhong University of Science and Technology, Wuhan 430074, PR China;

    Key Lab for Green Processing and Functionalization of New Textile Materials, Ministry of Education, Wuhan Textile University, Wuhan 430073, PR China;

    Key Lab for Green Processing and Functionalization of New Textile Materials, Ministry of Education, Wuhan Textile University, Wuhan 430073, PR China;

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  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    microwave sintering zno gas sensor impedance spectroscopy;

    机译:微波烧结zno气体传感器阻抗谱;

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