Intra-and Inter-Day Variation of LTE_4 Levels in Healthy Human Urine Using the Liquid Chromatography/Tandem Mass Spectrometric Method

Naoto Suzuki; Takanori Hishinuma; Michinao Mizugaki

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Intra-and Inter-Day Variation of LTE_4 Levels in Healthy Human Urine Using the Liquid Chromatography/Tandem Mass Spectrometric Method

机译：液相色谱/串联质谱法测定健康人尿中LTE_4水平的日内和日间变化

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Urinary leukotriene E_4 (LTE_4) levels in healthy volunteers were determined using liquid chromatography/ tandem mass spectrometry (LC/MS-MS). LTE_4 and its internal standard were extracted by simple solid-phase extraction and analyzed using LC/MS-MS in the selected reaction monitoring (SRM) model by monitoring the transitions between m/z 438 and m/z 333 for LTE_4 and between m/z 441 and m/z 336 for LTE_4-d_3.

机译：使用液相色谱/串联质谱法（LC / MS-MS）测定健康志愿者的尿白三烯E_4（LTE_4）水平。通过简单的固相萃取来提取LTE_4及其内标，并在LC / MS-MS中通过监测LTE_4在m / z 438和m / z 333之间以及在m / z 333和m / z 333之间的转换，在选定的反应监测（SRM）模型中进行分析。 LTE_4-d_3的z 441和m / z 336。

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《Journal of the Mass Spectrometry Society of Japan》 |2000年第2期|p.145-149|共5页
作者
Naoto Suzuki; Takanori Hishinuma; Michinao Mizugaki;
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正文语种 jpn
中图分类分析化学;一般工业技术;
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1. Intra-and Inter-Day Variation of LTE_4 Levels in Healthy Human Urine Using the Liquid Chromatography/Tandem Mass Spectrometric Method [J] . Naoto Suzuki, Takanori Hishinuma, Michinao Mizugaki Journal of the Mass Spectrometry Society of Japan . 2000,第2期

机译：液相色谱/串联质谱法测定健康人尿中LTE_4水平的日内和日间变化
2. A revised method for determination of dialkylphosphate levels in human urine by solid-phase extraction and liquid chromatography with tandem mass spectrometry: application to human urine samples from Japanese children [J] . Jun Ueyama, Isao Saito, Ayuko Takaishi, Environmental health and preventive medicine . 2014,第6期

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3. Development of high-performance liquid chromatography tandem mass spectrometric methods for the determination of a new oxytocin receptor antagonist (L-368,899) extracted from human plasma and urine: a case of lack of specificity due to the presence o [J] . Matuszewski BK., Constanzer ML., Chavez-Eng CM. Journal of Chromatography, Biomedical Applications . 1998,第1a2期

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6. A revised method for determination of dialkylphosphate levels in human urine by solid-phase extraction and liquid chromatography with tandem mass spectrometry: application to human urine samples from Japanese children [O] . Jun Ueyama, Isao Saito, Ayuko Takaishi, 2014

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机译：液相色谱的发展;电喷雾电离;串联mass211光谱法测定211人体内苯的尿代谢物

Intra-and Inter-Day Variation of LTE_4 Levels in Healthy Human Urine Using the Liquid Chromatography/Tandem Mass Spectrometric Method

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