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Production of Micro- and Nanofibrillated Cellulose through an Aqueous Counter Collision System Followed by Ultrasound: Effect of Mechanical Pretreatments

机译:通过抗撞机碰撞系统生产微型和纳米纤维纤维素,然后进行超声波:机械预处理的影响

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The purpose of this work was the production of cellulose micro-nanofibrils from wood pulps through a combination of mechanical treatments, including a recently patented process, a so-called aqueous counter collision (ACC) method followed by ultrasound treatment. Previously to ACC process, the raw pulp materials had to be downscaled to micro-sized dimension, due to the limits of collision jets nozzle diameter. Therefore, the softwood and hardwood pulps were mechanically pre-treated with valley beater refining or dry ball milling. Optical microscopy, atomic force microscopy, X-ray diffraction, thermogravimetric analysis, and gravimetric yield were estimated, to evaluate the effect of mechanical pretreatments on the proposed integrated fibrillation process. The characterizations indicated that valley beater as mechanical pretreatment was found to be more efficient compared to ball milling, of producing cellulose micro-nanofibrils in compliance with the proposed experimental procedure.
机译:这项工作的目的是通过机械处理的组合,包括最近获得专利的方法,即所谓的水上反碰撞(ACC)方法,其产生纤维素微纳米纤维,其次是超声处理。以前在ACC工艺中,由于碰撞喷嘴喷嘴直径的限制,原始纸浆材料必须落在微大尺寸上。因此,用谷搅拌器精炼或干球磨机械地预处理软木和硬木纸浆。估计光学显微镜,原子力显微镜,X射线衍射,热量分析和重力产量,以评估机械预处理对所提出的综合原纤化过程的影响。表征表明,与球磨相比,谷馒头作为机械预处理的效率更有效,并符合拟议的实验程序,产生纤维素微纳米纤维。

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