90‐kilobar diamond‐anvil high‐pressure cell for use on an automatic diffractometer

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90‐kilobar diamond‐anvil high‐pressure cell for use on an automatic diffractometer

机译：90千巴金刚石砧高压力池，用于自动衍射仪

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A gasketed diamond‐anvil high‐pressure cell is described which can be used on a four‐circle automatic diffractometer to collect x‐ray intensity data from single‐crystal samples subjected to truly hydrostatic pressures of over 90 kilobars. The force generating system exerts only forces normal to the diamond faces to obtain maximum reliability. A unique design allows exceptionally large open areas for maximum x‐ray access and is particularly well suited for highly absorbing materials, as the x rays are not transmitted through the sample. Studies on ruby show that high‐pressure crystal structure determinations may be done rapidly, reliably, and routinely with this system.

机译：描述了一种带垫片的金刚石-砧高压单元，该单元可用于四圆自动衍射仪上，以收集承受真正静水压超过90千巴的单晶样品的X射线强度数据。力产生系统仅施加垂直于金刚石面的力以获得最大的可靠性。独特的设计可提供超大的开放区域，以最大程度地获取X射线，并且特别适合高吸收性材料，因为X射线不会透过样品。对红宝石的研究表明，使用该系统可以快速，可靠且常规地确定高压晶体结构。

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《Review of Scientific Instruments》 |1978年第3期|P.359-364|共6页
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1. Laser heating in the diamond anvil press up to 2000°C sustained and 3000°C pulsed at pressures up to 260 kilobars [J] . Review of Scientific Instruments . 1974,第9期

机译：金刚石砧压机中的激光加热持续高达2000°C，并在高达260千巴的压力下以脉冲方式加热3000°C
2. The Accuracy of Diffraction Patterns Taken in a Diamond-Anvil Cell Using an X-ray Diffractometer According to the Dobrovol'skii-Shvedov Method [J] . N. V. Novikov, Yu. N. Krivosheya, L. K. Shvedov Journal of superhard materials: Sverkhtverdye materialy . 2013,第3期

机译：根据Dobrovol'skii-Shvedov方法使用X射线衍射仪在金刚石-砧座单元中获取衍射图的准确性
3. Pressure estimation using the 'diamond Raman scale' at low pressures in diamond anvil cell experiments using a highly confocal Raman system [J] . Fujii Taku, Ohfuji Hiroaki Measurement Science & Technology . 2015,第2期

机译：使用高度共聚焦的拉曼系统在金刚石砧室实验中使用低压“金刚石拉曼标尺”进行压力估算
4. The Hydrothermal Diamond Anvil Cell (HDAC) for Raman spectroseopic studies of geological fluids at high pressures and temperatures [C] . Christian SCHMIDT, I-Ming CHOU European Mineraligical Union School . 2012

机译：用于高压和温度下地质液的拉曼光谱研究的热热金刚石砧座（HDAC）
5. NMR experiments in a diamond anvil cell at high pressures. [D] . Pravica, Michael Gojko. 1998

机译：在高压下在钻石砧室中进行NMR实验。
6. Pressure Self-focusing Effect and Novel Methods for Increasing the Maximum Pressure in Traditional and Rotational Diamond Anvil Cells [O] . Biao Feng, Valery I. Levitas -1

机译：压力自聚焦效应和提高传统和旋转金刚石砧座细胞最大压力的新方法
7. Cryogenic Loading of Argon Pressure Medium in Diamond Anvil High Pressure Cells with in-situ Pressure Determination [O] . Pugh, Emma 2017

机译：原位测定法测定金刚石砧高压电池中氩压力介质的低温负荷
8. High Pressure X-Ray Studies of Polymers. I. Pressure Calibration for the Diamond Anvil-Cell in the Range 0-15 kbars. [R] . Sham, T. P., Newman, B. A., Pae, K. D. 1976

机译：聚合物的高压X射线研究。 I. 0-15 kbar范围内的金刚石砧座的压力校准。

90‐kilobar diamond‐anvil high‐pressure cell for use on an automatic diffractometer

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