Electrochemical Intercalation of ZnCl_2-CrO_3-GIC Graphite Intercalation Compound) with Sulphuric Acid

J.M.Skowronski; J.Urbaniak

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Electrochemical Intercalation of ZnCl_2-CrO_3-GIC Graphite Intercalation Compound) with Sulphuric Acid

机译：硫酸对ZnCl_2-CrO_3-GIC石墨插层化合物的电化学插层

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The intercalation processes of CrO_3 and H_2SO_4 into ZnCl_2-GIC have been confirmed by X-ray diffraction analysis and voltammetric technique.The proposed mechanism of the intercalation of ZnCl_2-GIC with CrO_3 assumes the formation of co-intercalation domains within the interlayer spacings of the graphite structure.Upon the successive intercalation of the graphite compound with H_2SO_4,the peaks characteristic of ZnCl_2 and CrO_3 have been observed in the voltammogram.This is an evidence of the formation of quaternary ZnCl_2-CrO_3-H_2SO_4-GIC.

机译：通过X射线衍射分析和伏安技术证实了CrO_3和H_2SO_4嵌入ZnCl_2-GIC的过程。拟议的ZnCl_2-GIC与CrO_3的嵌入机理是假设在CrO_3的层间间隔内形成共嵌入域石墨结构。在石墨化合物与H_2SO_4的连续插入后，在伏安图中观察到ZnCl_2和CrO_3的峰特征，这表明形成了ZnCl_2-CrO_3-H_2SO_4-GIC季铵盐。

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《Polish Journal of Chemistry》 |2004年第9期|共6页
作者
J.M.Skowronski; J.Urbaniak;
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正文语种 eng
中图分类化学;
关键词
graphite intercalation compounds; bi-intercalation; electrochemical properties; zinc chloride; chromium(VI) oxide; sulphuric acid;

机译：石墨插层化合物;双插层;电化学性能;氯化锌;氧化铬（VI）;硫酸;

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1. Electrochemical Intercalation of ZnCl_2-CrO_3-GIC Graphite Intercalation Compound) with Sulphuric Acid [J] . J.M.Skowronski, J.Urbaniak Polish Journal of Chemistry . 2004,第9期

机译：硫酸对ZnCl_2-CrO_3-GIC石墨插层化合物的电化学插层
2. Electrochemical intercalation of sulphuric acid into graphite in the presence of molybdenum trioxide [J] . Skowronski JM. Solid state ionics . 2003,第1a4期

机译：在三氧化钼存在下将硫酸电化学嵌入石墨中
3. Thermal exfoliation of electrochemically synthesized graphite intercalation compound with perrhenic acid [J] . Journal of solid state electrochemistry . 2020,第6期

机译：电化学合成石墨嵌入化合物与渗漏的热剥离
4. THE NATURE OF FLUORINE BONDS IN FLUORINATED CARBONS AND XPS STUDIES OF THE GRAPHITE OXIDE INTERCALATION COMPOUNDS WITH DODECAHEDRO-CLOSO-DODECABORIC ACID AND GRAPHITE NITRATE [C] . Yu.M. Nikolenko, V.I. Saldin, N.M. Mishchenko, EUROCARBON 2000 . 2000

机译：氟化碳中氟键的性质和XPS研究十二碳-十二碳-十二硼酸和硝酸石墨夹层化合物
5. Electrochemical synthesis of graphite intercalation compounds with low- or non-sulfur content. [D] . Kang, Feiyu. 1997

机译：低硫或无硫含量的石墨插层化合物的电化学合成。
6. The effect of graphite intercalated compound particle size and exfoliation temperature on porosity and macromolecular diffusion in expanded graphite [O] . R. Goudarzi, G. Hashemi Motlagh 2019

机译：石墨插层化合物的粒径和剥落温度对膨胀石墨中孔隙率和大分子扩散的影响
7. Electrochemical Reduction of Graphite Intercalation Compound with Sulfuric Acid Synthesized by Chemical Oxidation. [O] . Norio Iwashita, Michio Inagaki 1990

机译：用化学氧化合成石墨嵌入化合物的电化学还原。

Electrochemical Intercalation of ZnCl_2-CrO_3-GIC Graphite Intercalation Compound) with Sulphuric Acid

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