Synthesis and X-ray structure of a complex containing the trisimido borate trianion - the imido analogue of the orthoborate trianion

Jeffery JC.; Leedham AP.; Russell CA.

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Synthesis and X-ray structure of a complex containing the trisimido borate trianion - the imido analogue of the orthoborate trianion

机译：含三酰亚胺硼酸三阴离子的复合物的合成和X射线结构-原硼酸三阴离子的亚氨基类似物

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Reaction of BCl3 with 2-methoxyaniline (1:6 equiv.) in toluene, and subsequent metallation with (BuLi)-Bu-n (3 equiv.) produces {[Li4B(NR)(3)(THF)-T-.] (1) [(BBu4)-Bu-n] (.)toluene}(2) (R = 2-methoxyphenyl), which contains the first example of a trisimido borate trianion-the imido analogue of the orthoborate trianion, [BO3](3-). (C) 2002 Elsevier Science Ltd. All rights reserved. [References: 23]

机译：使BCl3与2-甲氧基苯胺（1：6当量）在甲苯中反应，然后与（BuLi）-Bu-n（3当量）进行金属化反应，生成{[Li4B（NR）（3）（THF）-T-。 ]（1）[（BBu4）-Bu-n]（。）甲苯}（2）（R = 2-甲氧基苯基），其中包含三酰亚胺硼酸酯三阴离子的第一个例子-原硼酸三阴离子的酰亚胺类似物[BO3 ]（3-）。（C）2002 Elsevier ScienceLtd。保留所有权利。 [参考：23]

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《Polyhedron: The International Journal for Inorganic and Organometallic Chemistry》 |2002年第6期|共4页
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Jeffery JC.; Leedham AP.; Russell CA.;
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中图分类化学;无机化学;
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1. Synthesis and X-ray structure of a complex containing the trisimido borate trianion - the imido analogue of the orthoborate trianion [J] . Jeffery JC., Leedham AP., Russell CA. Polyhedron: The International Journal for Inorganic and Organometallic Chemistry . 2002,第5a6期

机译：含三酰亚胺硼酸三阴离子的复合物的合成和X射线结构-原硼酸三阴离子的亚氨基类似物
2. Synthesis and X-ray structure of the [{Fe-3(CO)(9)(mu(3)-O)}(2)H](3-) trianion: dimerization of a metal carbonyl cluster via formation of an exceptionally short hydrogen bond [J] . Femoni C, Iapalucci MC, Longoni G, Dalton transactions: An international journal of inorganic chemistry . 2007,第25期

机译：[{Fe-3（CO）（9）（mu（3）-O）}（2）H]（3-）三阴离子的合成和X射线结构：羰基金属簇的形成通过异常形成的二聚作用短氢键
3. Synthesis, spectroscopic characterization and X-ray crystal structures of oxo-bridged oxo(haloaryl) imido hydrotris(3,5-dimethylpyrazolyl)borate molybdenum(V) complexes [J] . ISIL TOPALOGLU-SOZUER, SECKINER DULGER IRDEM, JOHN J. JEFFERY Journal of Coordination Chemistry . 2005,第2期

机译：羰基桥联的氧代（卤代芳基）亚氨基氢三（3,5-二甲基吡唑基）硼酸钼（V）配合物的合成，光谱表征和X射线晶体结构
4. Synthesis,Structures,and Reactivity of Rare Earth Imido Complexes Bearing Monocyclopentadienyl Ligands [C] . Masavoshi Nishiura, Dongmei Cui, Olivier Tardif, Symposium on Organometallic Chemistry . 2003

机译：稀土咪啶配合物含有单环戊二烯基配体的合成，结构和反应性
5. SYNTHESIS AND CHEMISTRY OF CARBONYLMETALLATE TRIANIONS OF VANADIUM, NIOBIUM, TANTALUM, MANGANESE, RHENIUM, COBALT AND IRIDIUM. PART ONE: THE CHEMISTRY OF THE PENTACARBONYLMETALLATE TRIANIONS OF VANADIUM, NIOBIUM AND TANTALUM. PART TWO: THE CHEMISTRY OF THE TETRACARBONYLMETALLATE TRIANIONS OF MANGANESE AND RHENIUM. PART THREE: THE CHEMISTRY OF THE TRICARBONYLMETALLATE TRIANIONS OF COBALT AND IRIDIUM. [D] . WARNOCK, GARRY FRANCIS. 1985

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6. Total Synthesis of Lepadiformine Alkaloids using N-Boc α-Amino Nitriles as Trianion Synthons [O] . Matthew A. Perry, Matthew D. Morin, Brian W. Slafer, -1

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7. Synthesis, spectroscopic characterization and X-ray crystal structures of oxo-bridged oxo(haloaryl) imido hydrotris(3,5-dimethylpyrazolyl)borate molybdenum(V) complexes [O] . Sözüer Hikmet Işıl, İrdem Seçkiner Dülgel, Jeffery John J., 2005

机译：羰基桥联的氧代（卤代芳基）亚氨基氢三（3，5-二甲基吡唑基）硼酸钼（V）配合物的合成，光谱表征和X射线晶体结构
8. Synthesis of a Boron Analogue of Co-Ordinated Cyclobutadiene; X-Ray Molecular Structures of Closo- and Nido-L2PtC2B6H6R2. [R] . Green, M., Spencer, J. L., Stone, F. G. A., 1974

机译：共聚环己二烯的硼类似物的合成; Closo-和Nido-L2ptC2B6H6R2的X射线分子结构。

Synthesis and X-ray structure of a complex containing the trisimido borate trianion - the imido analogue of the orthoborate trianion

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