Iron(III) mixed-ligand complexes: Synthesis, characterization and crystal structure determination of iron(III) hetero-ligand complexes containing 1,10-phenanthroline, 2,2 '-bipyridine, chloride and dimethyl sulfoxide, [Fe(phen)Cl-3(DMSO)] and [Fe(bip

Amani V; Safari N; Khavasi HR; Mirzaei P

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Iron(III) mixed-ligand complexes: Synthesis, characterization and crystal structure determination of iron(III) hetero-ligand complexes containing 1,10-phenanthroline, 2,2 '-bipyridine, chloride and dimethyl sulfoxide, [Fe(phen)Cl-3(DMSO)] and [Fe(bip

机译：铁（III）混合配体配合物：含1,10-菲咯啉，2,2'-联吡啶，氯化物和二甲基亚砜，[Fe（phen）Cl]的铁（III）杂配体配合物的合成，表征和晶体结构测定-3（DMSO）]和[Fe（bip

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Treatment of [Fe(bipy)Cl-4][bipy center dot H] (1) and [Fe(phen)Cl-4][phen center dot H] (3) (where bipy is 2,2'-bipyridine and phen is 1,10-phenanthroline) with dimethyl sulfoxide in methanolic solution produced [Fe(bipy)Cl-3(DMSO)] (2) and [Fe(phen)Cl-3(DMSO)] (4) (where DMSO is dimethyl sulfoxide), respectively. The resulting complexes were characterized by elemental analysis, IR, UV-Vis and H-1 NMR spectroscopies and by the X-ray diffraction method. These complexes are high spin with a spin multiplicity of 6. (C) 2007 Elsevier Ltd. All rights reserved.

机译：[Fe（bipy）Cl-4] [bipy中心点H]（1）的处理（其中bipy是2,2'-联吡啶和phen是1,10-菲咯啉）与二甲亚砜在甲醇溶液中制得的[Fe（bipy）Cl-3（DMSO）]（2）和[Fe（phen）Cl-3（DMSO）]（4）（其中DMSO是二甲基亚砜）。通过元素分析，IR，UV-Vis和H-1 NMR光谱以及X射线衍射法对所得复合物进行表征。这些复合物具有6的自旋多重性。（C）2007 Elsevier Ltd.保留所有权利。

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《Polyhedron: The International Journal for Inorganic and Organometallic Chemistry》 |2007年第17期|共7页
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Amani V; Safari N; Khavasi HR; Mirzaei P;
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正文语种 eng
中图分类化学;
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iron(III); 2; 2 '-bipyridine; 1; 10-phenanthroline; chloride; dimethyl sulfoxide; crystal structure; TRANSITION-METAL COMPLEXES; ELECTROCHEMICAL POLYMERIZATION; ALPHA; ALPHA'-DIIMINE SYSTEM; LUMINESCENT; FILMS; RESONANCE; OXIDATION; PROPERTY;

机译：铁（III）;2;2'-联吡啶;1;10-菲咯啉;氯化物;二甲亚砜;晶体结构;过渡金属配合物;电化学聚合;阿尔法;阿尔法-二亚胺体系;发光率;薄膜;共振;氧化;属性;

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Iron(III) mixed-ligand complexes: Synthesis, characterization and crystal structure determination of iron(III) hetero-ligand complexes containing 1,10-phenanthroline, 2,2 '-bipyridine, chloride and dimethyl sulfoxide, [Fe(phen)Cl-3(DMSO)] and [Fe(bip

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