Ionothermal Synthesis of Crystalline, Condensed, Graphitic Carbon Nitride

Bojdys MJ; Muller JO; Antonietti M; Thomas A

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Ionothermal Synthesis of Crystalline, Condensed, Graphitic Carbon Nitride

机译：离子热合成结晶，缩合，石墨化氮化碳

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Herein we report the synthesis of a crystalline graphitic carbon nitride, or g-C3N4, obtained from the temperature-induced condensation of dicyandiamide (NH2C(=NH)NHCN) by using a salt melt of lithium chloride and potassium chloride as the solvent. The proposed crystal structure of this g-C3N4 species is based on sheets of hexagonally arranged s-heptazine (C6N7) units that are held together by covalent bonds between C and N atoms which are stacked in a graphitic, staggered fashion, as corroborated by powder X-ray diffractometry and high-resolution transmission electron microscopy.

机译：在这里，我们报道了通过使用氯化锂和氯化钾的盐熔体作为溶剂，通过温度诱导的双氰胺（NH2C（= NH）NHCN）的缩合反应获得的结晶石墨碳氮化物或g-C3N4的合成。此g-C3N4物种的拟议晶体结构是基于六边形排列的s-庚嗪（C6N7）单元片，这些单元通过C和N原子之间的共价键保持在一起，并以石墨，交错的方式堆叠，并得到粉末的证实。 X射线衍射仪和高分辨率透射电子显微镜。

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《Chemistry: A European journal》 |2008年第27期|共6页
作者
Bojdys MJ; Muller JO; Antonietti M; Thomas A;
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正文语种 eng
中图分类化学;
关键词
carbon nitrides; covalent frameworks; layered compounds; salt melt; solid-state structures; S-TRIAZINE DERIVATIVES; CHEMICAL-SYNTHESIS; C3N4; ACTIVATION; PRECURSORS; BENZENE; SALTS;

机译：碳氮化物;共价骨架;层状化合物;盐熔体;固态结构;S-三嗪衍生物;化学合成;C3N4;活化;前体;苯;盐;

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1. Ionothermal Synthesis of Crystalline, Condensed, Graphitic Carbon Nitride [J] . Bojdys MJ, Muller JO, Antonietti M, Chemistry: A European journal . 2008,第27期

机译：离子热合成结晶，缩合，石墨化氮化碳
2. Condensed and low-defected graphitic carbon nitride with enhanced photocatalytic hydrogen evolution under visible light irradiation [J] . Cui Yanjuan, Zhang Guigang, Lin Zhenzhen, Applied Catalysis, B. Environmental: An International Journal Devoted to Catalytic Science and Its Applications . 2016,第Null期

机译：在可见光照射下具有增强的光催化氢释放作用的凝聚和低挠曲石墨氮化碳
3. Cu-doped carbon nitride: Bio-inspired synthesis of H-2-evolving electrocatalysts using graphitic carbon nitride (g-C3N4) as a host material [J] . Zou Xiaoxin, Silva Rafael, Goswami Anandarup, Applied Surface Science . 2015,第DECa1PTaA期

机译：掺杂铜的氮化碳：以石墨化氮化碳（g-C3N4）为主体材料，生物启发的H-2进化电催化剂的合成
4. The Synthesis, Characterization and Visible-Light Photodegradation Performance of Graphitic Carbon Nitride Coupling with CoAPO-5 [C] . Zhiwei Zhou, Lingfang Qiu, Xiaobin Qiu, China international conference on high-performance ceramics . 2018

机译：咖啡-5与石墨氮化物偶联的合成，表征和可见光光降解性能
5. Rapid solid-state synthesis of group 6 nitrides, carbon nanotubes and graphite-encapsulated metal nanoparticles. [D] . O'Loughlin, Jennifer Leigh. 2000

机译：快速固态合成第6组氮化物，碳纳米管和石墨包裹的金属纳米颗粒。
6. Graphitic Carbon Nitride Nanosheets Covalently Functionalizedwith Biocompatible Vitamin B1: Synthesis Characterizationand Its Superior Performance for Synthesis of Quinoxalines [O] . Afsaneh Rashidizadeh, Hossein Ghafuri, *, 2019

机译：石墨碳氮化物纳米片共价功能化与生物相容性维生素B1的合成表征及其合成喹喔啉的优异性能
7. Direct Synthesis of O-doped Carbon Nitride and Oxide of Graphite-like Carbon Nitride from Melamine [O] . Kharlamov A.I., Bondarenko M.E., Kharlamova G.A., 2015

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Ionothermal Synthesis of Crystalline, Condensed, Graphitic Carbon Nitride

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