Synthesis of Scroll-Type Composite Microtubes of Mo_2C/MoCO by Controlled Pyrolysis of Mo(CO)_6

Xiao-Lin Li; Ya-Dong Li

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Synthesis of Scroll-Type Composite Microtubes of Mo_2C/MoCO by Controlled Pyrolysis of Mo(CO)_6

机译：Mo（CO）_6的控制热解合成Mo_2C / MoCO涡旋型复合微管

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Composite microtubes of Mo_2C/MoCO have been synthesized for the first time under well-controlled conditions by thermal decomposition of Mo(CO)_6 at about 600 deg C.Here,thermall stability and phase transition of the products,as well as the influence of reaction temperature and argon flow rate,have been carefully investigated.All samples were characterized by X-ray powder diffraction (XRD),scanning electron microscopy (SEM),and X-ray photoelectron spectroscopy (XPS).The reaction model and rolling mechanism were proposed on the basis of the experimental facts.

机译：Mo_2C / MoCO复合微管是在良好控制的条件下通过在约600℃左右热分解Mo（CO）_6首次合成的。在此，产物的热稳定性和相变以及仔细研究了反应温度和氩气流速。对所有样品进行了X射线粉末衍射（XRD），扫描电子显微镜（SEM）和X射线光电子能谱（XPS）表征。根据实验事实提出。

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《Chemistry: A European journal》 |2004年第2期|共7页
作者
Xiao-Lin Li; Ya-Dong Li;
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正文语种 eng
中图分类化学;
关键词
carbides; microtubes; molybdenum; scanning probe microscopy; X-ray diffraction;

机译：碳化物;微管;钼;扫描探针显微镜;X射线衍射;

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专利

1. Synthesis of Scroll-Type Composite Microtubes of Mo_2C/MoCO by Controlled Pyrolysis of Mo(CO)_6 [J] . Xiao-Lin Li, Ya-Dong Li Chemistry: A European journal . 2004,第2期

机译：Mo（CO）_6的控制热解合成Mo_2C / MoCO涡旋型复合微管
2. Synthesis of a (MoSi_2, Mo_5Si_3)/SiC Composite Using an In Situ Solid-State Desplacement Reaction between Mo_2C and Si [J] . Francisco Javier NARCISO-ROMERO, Roberto APPON-CARBALLO 日本セラミックス協会学術論文誌 . 2000,第1263期

机译：使用Mo_2C和Si之间的原位固态去移反应合成（MOSI_2，MO_5SI_3）/ SIC复合材料
3. One-Step Synthesis of TiO2/Graphene Nanocomposites by Laser Pyrolysis with Well-Controlled Properties and Application in Perovskite Solar Cells [J] . Rapha?lle Belchi, Aurélie Habert, Eddy Foy, ACS Omega . 2019,第7期

机译：用良好控制性能激光热解的TiO2 /石墨烯纳米复合物的一步合成及在钙钛矿太阳能电池中的应用
4. Synthesis of Nanosized Nitrogen-containing MO_x-ZnO (M= W, V, Fe) Composite Powders by Spray Pyrolysis and Their Photocatalysis in the Gas-phase Acetaldehyde Decomposition [C] . D. Li, N. Saito N. Ohashi, S. Hishita, Asia-Pacific Congress on Catalysis . 2003

机译：通过喷雾热解及其光催化在气相乙醛分解中通过喷雾热解合成纳米氧化氮MO_X-ZnO（M = W，V，Fe）复合粉末
5. Liquid-feed flame spray pyrolysis synthesis of oxide nanopowders for the processing of ceramic composites. [D] . Taylor, Nathan John. 2015

机译：液体进料火焰喷雾热解法合成氧化物纳米粉体，用于陶瓷复合材料的加工。
6. One-Step Synthesis of TiO2/Graphene Nanocompositesby Laser Pyrolysis with Well-Controlled Properties and Applicationin Perovskite Solar Cells [O] . Raphaëlle Belchi, Aurélie Habert, Eddy Foy, 2019

机译：一步法合成TiO2 /石墨烯纳米复合材料性能良好的激光热解法制备及应用在钙钛矿太阳能电池中
7. Facile Synthesis and Characterization of Few-Layer Multifunctional Graphene from Sustainable Precursors by Controlled Pyrolysis, Understanding of the Graphitization Pathway, and Its Potential Application in Polymer Nanocomposites [O] . Amrita Roy, Saptarshi Kar, Ranjan Ghosal, 2021

机译：通过受控热解，理解石墨化途径的可持续前体少层多官能石墨烯的构成与表征及其在聚合物纳米复合材料中的潜在应用
8. The universal applications of microtubes and microtube composites [R] . Hoffman, Wesley P., Upadhya, Kamleshwar 1994

机译：微管和微管复合材料的普遍应用

Synthesis of Scroll-Type Composite Microtubes of Mo_2C/MoCO by Controlled Pyrolysis of Mo(CO)_6

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