Tag-Reporter and Resin Capture-Release Strategy in Oligosaccharide Synthesis

Yukishige Ito; Shino Manabe

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Tag-Reporter and Resin Capture-Release Strategy in Oligosaccharide Synthesis

机译：寡糖合成中的Tag-Reporter和树脂捕获-释放策略

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Low molecular weight poly (ethylene glycol) (LWPEG) has been found to be useful as a "tag" in oligosaccharide synthesis due to its high polarity. Realtime reaction monitoring was achieved by use of MAL-DI-TOF MS in the glycosylation reactions and color tests in the deprotection of the chloroacetyl group. Further, a cysteine-supported insoluble resin enables the purification of the chloroacetyl-bound compounds on soluble PEG.

机译：已经发现低分子量聚（乙二醇）（LWPEG）由于其高极性而在寡糖合成中用作“标签”。通过在糖基化反应中使用MAL-DI-TOF MS和在氯乙酰基脱保护中进行颜色测试来实现实时反应监控。此外，半胱氨酸负载的不溶性树脂能够纯化在可溶性PEG上结合氯乙酰基的化合物。

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《Chemistry: A European journal》 |2002年第14期|共8页
作者
Yukishige Ito; Shino Manabe;
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正文语种 eng
中图分类化学;应用化学;
关键词
capture-release purification; oligosaccharides; polymer-supported synthesis; real-time monitoring; synthesis design;

机译：捕获释放纯化;低聚糖;聚合物支持的合成;实时监测;合成设计;

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专利

1. Tag-Reporter and Resin Capture-Release Strategy in Oligosaccharide Synthesis [J] . Yukishige Ito, Shino Manabe Chemistry: A European journal . 2002,第14期

机译：寡糖合成中的Tag-Reporter和树脂捕获-释放策略
2. Solid-phase capture-release strategy applied to oligosaccharide synthesis on a soluble polymer support [J] . Hiromune Ando, Shino Manabe, Yoshiaki Nakahara, Chembiochem: A European journal of chemical biology . 2001,第24期

机译：固相捕获-释放策略应用于可溶性聚合物载体上的寡糖合成
3. Divergent Synthesis of Sialylated Glycan Chains:Combined Use of Polymer Support,Resin Capture-Release,and Chemoenzymatic Strategies [J] . Shinya Hanashima, Shino Manabe, Yukishige Ito Angewandte Chemie . 2005,第27期

机译：唾液酸化糖链的不同合成：聚合物载体，树脂捕获-释放和化学酶策略的组合使用
4. Strategies for Synthesis of an Oligosaccharide Library Using a Chemoenzymatic Approach [C] . Ola Blixt, Nahid Razi American Chemical Society Meeting . 2004

机译：使用化学酶方法合成寡糖文库的策略
5. Part I. Synthesis and conformational analysis of 6- C-methyl substituted 2-acetamido-2-deoxy-beta-D-glucopyranosides. Part II. Design and strategies towards a unified synthesis of heparan sulfate oligosaccharides. [D] . Achkar, Jihane. 2003

机译：第一部分：6-C-甲基取代的2-乙酰氨基-2-脱氧-β-D-吡喃葡萄糖苷的合成和构象分析。第二部分统一合成硫酸乙酰肝素寡糖的设计和策略。
6. On-resin Convergent Synthesis of a Glycopeptide from HIV gp120 Containing a High Mannose N-linked Oligosaccharide [O] . Rui Chen, Thomas J. Tolbert -1

机译：含有高甘露糖N-连接寡糖的HIV GP120的树脂肽的合成糖肽
7. Chemical Synthesis of Bioactive Oligosaccharides. Synthetic Studies on Resin Glycosides. [O] . Jun-ichi Furukawa, Nobuo Sakairi 2001

机译：生物活性寡糖的化学合成。树脂糖苷的合成研究。

Tag-Reporter and Resin Capture-Release Strategy in Oligosaccharide Synthesis

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