Chemiluminescence detection of 1,3,5-trinitro-1,3,5-triazacyclohexane (RDX) and related nitramine explosives

Donaldson D.N.; Barnett N.W.; Agg K.M.; Graham D.; Lenehan C.E.; Prior C.; Lim K.F.; Francis P.S.

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Chemiluminescence detection of 1,3,5-trinitro-1,3,5-triazacyclohexane (RDX) and related nitramine explosives

机译：1,3,5-三硝基-1,3,5-三氮杂环己烷（RDX）和相关硝胺炸药的化学发光检测

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A simple controlled chemical reduction of 1,3,5-trinitro-1,3,5- triazacyclohexane (RDX) and related nitramine compounds with zinc amalgam generates species that elicit intense chemiluminescence with tris(2,2′-bipyridine)ruthenium(III), which extends this widely utilised chemiluminescence reagent to a new class of analyte and presents a sound chemical basis for a screening test for nitramine high explosives. Examination of the chemiluminescence profiles under stopped-flow conditions revealed contributions from multiple transient species formed in the initial reduction step.

机译：用锌汞合金对1,3,5-三硝基-1,3,5-三氮杂环己烷（RDX）和相关的硝胺化合物进行简单的受控化学还原，会生成引发三（2,2'-联吡啶）钌（III）强烈化学发光的物质），将这种广泛使用的化学发光试剂扩展到一类新的分析物，并为硝胺高炸药的筛选测试提供了良好的化学基础。在停止流动条件下检查化学发光曲线表明，在初始还原步骤中形成了多种瞬态物质。

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《Talanta: The International Journal of Pure and Applied Analytical Chemistry》 |2012年第null期|共6页
作者
Donaldson D.N.; Barnett N.W.; Agg K.M.; Graham D.; Lenehan C.E.; Prior C.; Lim K.F.; Francis P.S.;
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正文语种 eng
中图分类分析化学;
关键词
Chemiluminescence detection; Cyclotrimethylenetrinitramine; Flow injection analysis; Nitramine explosive; Ruthenium complexes;

机译：化学发光检测环三亚甲基三硝胺流动注射分析硝胺炸药钌配合物;

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1. Chemiluminescence detection of 1,3,5-trinitro-1,3,5-triazacyclohexane (RDX) and related nitramine explosives [J] . Donaldson D.N., Barnett N.W., Agg K.M., Talanta: The International Journal of Pure and Applied Analytical Chemistry . 2012,第Null期

机译：1,3,5-三硝基-1,3,5-三氮杂环己烷（RDX）和相关硝胺炸药的化学发光检测
2. Clostridium geopurificans Strain MJ1 sp nov., A Strictly Anaerobic Bacterium that Grows via Fermentation and Reduces the Cyclic Nitramine Explosive Hexahydro-1,3,5-Trinitro-1,3,5-Triazine (RDX) [J] . Kwon Man Jae, Wei Na, Millerick Kayleigh, Current Microbiology: An International Journal . 2014,第6期

机译：梭状芽胞杆菌菌株MJ1 sp nov。，一种严格的厌氧细菌，可通过发酵生长并减少环硝胺爆炸性六氢-1,3,5-三硝基-1,3,5-三嗪（RDX）
3. Biochemical and Microbial Analysis of Ovine Rumen Fluid Incubated with 1,3,5-Trinitro-1,3,5-triazacyclohexane (RDX) [J] . Perumbakkam Sudeep, Craig A. Morrie Current Microbiology: An International Journal . 2012,第2期

机译：1,3,5-三硝基-1,3,5-三氮杂环己烷（RDX）培养的羊瘤胃液的生化和微生物分析
4. Thermal behavior of Hexanitrohexazaisowurtzitane /1,3,5-trinitro-1,3,5- triazacyclohexane binary system [C] . Zi-Ru Liu, Cui-Mei Yin, Yan Liu, Proceedings of the 31st annual conference of the North American Thermal Analysis Society(NATAS) . 2003

机译：六硝基六氮杂异纤锌矿型结构烷烃/ 1,3,5-三硝基-1,3,5-三氮杂环己烷二元体系的热行为
5. Biological treatment of 2,4,6-trinitrotoluene (TNT), hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX), and octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX), and the hydrolysates of RDX and HMX. [D] . Reinhart, George Albetz, III. 2001

机译：2,4,6-三硝基甲苯（TNT），六氢-1,3,5-三硝基-1,3,5-三嗪（RDX）和八氢-1,3,5,7-四硝基-1的生物处理， 3,5,7-四唑嗪（HMX），以及RDX和HMX的水解产物。
6. Mineralization of the Cyclic Nitramine Explosive Hexahydro-135-Trinitro-135-Triazine by Gordonia and Williamsia spp. [O] . Karen T. Thompson, Fiona H. Crocker, Herbert L. Fredrickson 2005

机译：Gordonia和Williamsia spp对环硝胺爆炸性六氢-135-三硝基-135-三嗪的矿化作用。
7. Mineralization of the Cyclic Nitramine Explosive Hexahydro-1,3,5-Trinitro-1,3,5-Triazine by Gordonia and Williamsia spp. [O] . Thompson, Karen T., Crocker, Fiona H., Fredrickson, Herbert L. 2005

机译：Gordonia和Williamsia spp对环硝胺爆炸性六氢-1,3,5-三硝基-1,3,5-三嗪的矿化作用。
8. Computational Study of the Concerted Gas Phase Triple Dissociations of 1,3,5-Triazacyclohexane and Its 1,3,5-Trinitro Derivative (RDX) [R] . Habibollahzadeh, D., Grodzicki, M., Seminario, J. M., 1991

机译：1,3,5-三氮杂环己烷及其1,3,5-三硝基衍生物（RDX）气相三相离解的计算研究

Chemiluminescence detection of 1,3,5-trinitro-1,3,5-triazacyclohexane (RDX) and related nitramine explosives

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