[3 + 2] Cycloaddition of Allylic Silane with N-Chlorosulfonyl Isocyanate

Masahiko Isaka; Paul G. Williard; Eiichi Nakamura

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[3 + 2] Cycloaddition of Allylic Silane with N-Chlorosulfonyl Isocyanate

机译：[3 + 2]烯丙基硅烷与N-氯磺酰基异氰酸酯的环加成反应

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摘要

Reaction of a substituted allylsilane with N-chlorosulfonyl isocyanate at 0 deg C takes place in an unexpected manner to give a [3 + 2] cycloaddition product, a #beta#-silyl-#gamma#-lactam, rather than a [2 + 2] cycloadduct.

机译：取代的烯丙基硅烷与N-氯磺酰基异氰酸酯在0℃发生意外反应，得到[3 + 2]环加成产物＃β＃-甲硅烷基-＃gamma＃-内酰胺，而不是[2+ 2]环加合物。

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《Bulletin of the Chemical Society of Japan》 |1999年第9期|共2页
作者
Masahiko Isaka; Paul G. Williard; Eiichi Nakamura;
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正文语种 eng
中图分类化学;化学工业;
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1. [3 + 2] Cycloaddition of Allylic Silane with N-Chlorosulfonyl Isocyanate [J] . Masahiko Isaka, Paul G. Williard, Eiichi Nakamura Bulletin of the Chemical Society of Japan . 1999,第9期

机译：[3 + 2]烯丙基硅烷与N-氯磺酰基异氰酸酯的环加成反应
2. Stereoselective synthesis of highly substituted gamma-lactams by the [3+2] annulation of alpha-siloxy allylic silanes with chlorosulfonyl isocyanate [J] . Romero A, Woerpel KA Organic letters . 2006,第10期

机译：通过[3 + 2]α-甲硅烷氧基烯丙基硅烷与氯磺酰基异氰酸酯的环化反应，立体选择性地合成高度取代的γ-内酰胺
3. Stereoselective Synthesis of Highly Substituted γ-Lactams by the [3+2] Annulation of α-Siloxy Allylic Silanes with Chlorosulfonyl Isocyanate [J] . Antonio Romero, K. A. Woerpel Organic letters . 2006,第10期

机译：[3 + 2]α-甲硅烷氧基烯丙基硅烷与氯磺酰基异氰酸酯的环化反应立体选择性合成高取代的γ-内酰胺
4. A Catalytic Asymmetric 1,3-Dipolar Cycloaddition of Nitrones to Allylic Alcohols [C] . Xia Ding 11th International Symposium of Fine Chemistry and Functional Polymers Jul 28-31, 2001 Hailar, Inner Mongolia, P.R. China . 2001

机译：氮到烯丙醇的催化不对称1,3-偶极环加成反应
5. Synthesis and structure-property studies of polysiloxane polyurethane isocyanate-functional polymeric silanes. [D] . Dai, Zhisheng. 1993

机译：聚硅氧烷聚氨酯异氰酸酯官能聚合硅烷的合成和结构性能研究。
6. Pd-Catalyzed Synthesis of Allylic Silanes from Allylic Ethers [O] . Ralph Moser, Takashi Nishikata, Bruce H. Lipshutz -1

机译：于烯丙基醚烯丙基硅烷的钯催化合成
7. Pd-Catalyzed Asymmetric Allylic Cycloaddition of NContaining Allylic Carbonates with Isocyanates [O] . -1

机译：用异氰酸酯催化NCOLICALLIC碳酸酯的PD催化的不对称烯丙基环加成

[3 + 2] Cycloaddition of Allylic Silane with N-Chlorosulfonyl Isocyanate

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