Low-Temperature Synthesis of Nanocrystalline ZrB_2 via Co-reduction of ZrCl_4 and BBr_3

Luyang Chen; Yunle Gu; Liang Shi

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Low-Temperature Synthesis of Nanocrystalline ZrB_2 via Co-reduction of ZrCl_4 and BBr_3

机译：通过共还原ZrCl_4和BBr_3低温合成纳米晶ZrB_2

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Nanocrystalline zirconium diboride (ZrB2) has been synthesized via a sodium co-reduction of ZrCl_4 and BBrs at 400 deg C.The XRD patterns can be indexed as hexagonal ZrB_2 with the lattice constants a = 3.167 and c = 3.527 A.The TEM image indicates the product has particle morphology,with size of about 20 nm.

机译：通过在400℃下钠共还原ZrCl_4和BBrs合成了纳米晶二硼化锆（ZrB2）.XRD图谱可以索引为六方晶ZrB_2，晶格常数a = 3.167和c = 3.527 A.TEM图像表明产品具有颗粒形态，尺寸约20 nm。

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《Bulletin of the Chemical Society of Japan》 |2004年第7期|共2页
作者
Luyang Chen; Yunle Gu; Liang Shi;
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中图分类化学;
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Low-Temperature Synthesis of Nanocrystalline ZrB_2 via Co-reduction of ZrCl_4 and BBr_3

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