Microwave-promoted automated synthesis of a coumarin library

M. Katkevics; A. Kontijevskis; I. Mutule; E. Suna

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Microwave-promoted automated synthesis of a coumarin library

机译：微波促进的香豆素文库的自动合成

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A 30-membered library of coumarins has been synthesized in a microwave-assisted Pechmann reaction using neat trifluoroacetic acid both as an acidic reagent and a reaction medium. Alternatively, polymer-supported sulfonic acid Amberlyst-15 could also be employed to facilitate the formation of coumarins. The use of a specially-built microwave synthesizer with liquid handling tools rendered the automated synthesis of a coumarin library feasible.

机译：使用纯净的三氟乙酸作为酸性试剂和反应介质，在微波辅助的Pechmann反应中合成了30个成员的香豆素文库。或者，也可以使用聚合物负载的磺酸Amberlyst-15来促进香豆素的形成。使用特殊的微波合成器和液体处理工具使香豆素库的自动合成成为可能。

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《Chemistry of heterocyclic compounds》 |2007年第2期|共9页
作者
M. Katkevics; A. Kontijevskis; I. Mutule; E. Suna;
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原文格式 PDF
正文语种 eng
中图分类杂环化合物;
关键词
coumarin; microwave promoted synthesis; library synthesis;

机译：香豆素;微波促进合成;文库合成;

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专利

1. Microwave-promoted automated synthesis of a coumarin library [J] . M. Katkevics, A. Kontijevskis, I. Mutule, Chemistry of heterocyclic compounds . 2007,第2期

机译：微波促进的香豆素文库的自动合成
2. Microwave-Promoted One-Pot Syntheses of Coumarin Dyes [J] . Synthetic Communications . 2010,第6期

机译：微波促进香豆素染料的一锅合成
3. MICROWAVE-PROMOTED ONE-POT SYNTHESES OF COUMARIN DYES [J] . Farahnaz Nourmohammadian, Mahnaz Davoodzadeh Gholami Synthetic Communications . 2010,第4a6期

机译：微波促进香豆素染料的一锅合成
4. Automated synthesis of cell libraries for asynchronous circuits [C] . Moreira Matheus Trevisan, Arendt Michel, Ziesemer Adriel, Symposium on Integrated Circuits and Systems Design . 2014

机译：自动合成异步电路的单元库
5. Coumarins, macrocycles, and indazoles: Solution and solid phase synthesis of libraries of biologically interesting heterocycles. [D] . Mills, Aaron. 2005

机译：香豆素，大环化合物和吲唑：具有生物学意义的杂环文库的溶液和固相合成。
6. Solution-phase Synthesis of a Combinatorial Library of 3-4-(Coumarin-3-yl)-13-thiazol-2-ylcarbamoylpropanoic acid Amides [O] . Irina O. Zhuravel, Sergiy M. Kovalenko, Sergiy V. Vlasov, 2005

机译：3- 4-（香豆素-3-基）-13-噻唑-2-基氨基甲酰基丙酸酰胺的组合库的溶液相合成
7. Solution-phase Synthesis of a Combinatorial Library of 3-[4-(Coumarin-3-yl)-1,3-thiazol-2-ylcarbamoyl]propanoic acid Amides [O] . V. Chernykh, S. Vlasov, S. Kovalenko, 2005

机译：溶液相合成3- [4-（香豆素-3-基）-1,3-噻唑-2-基氨基甲酰基]丙酸酰胺的组合文库

Microwave-promoted automated synthesis of a coumarin library

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