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首页> 外文期刊>The journal of physical chemistry, C. Nanomaterials and interfaces >Synthesis of Crystalline Microporous SnO2 via a Surfactant-Assisted Microwave Heating Method: A General and Rapid Method for the Synthesis of Metal Oxide Nanostructures
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Synthesis of Crystalline Microporous SnO2 via a Surfactant-Assisted Microwave Heating Method: A General and Rapid Method for the Synthesis of Metal Oxide Nanostructures

机译:通过表面活性剂辅助微波加热法合成结晶微孔SnO2:合成金属氧化物纳米结构的通用快速方法

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摘要

Although synthetic investigations of inorganic nanomaterials had been carried out extensively over the past decade, the rapid synthesis of crystalline microporous nanostructures with a high surface—volume ratio is still a significant challenge. In this work, by combining the excellent properties of both microwave heating and surfactant, we developed for the first time a novel surfactant-assisted microwave heating route for the rapid synthesis of crystalline microporous SnO2 with a very high sensitivity to ethanol. The formation mechanism of the as-prepared microporous SnO2 was been investigated and discussed in this paper. Furthermore, this synthetic route was shown to be a general and rapid method for the shape-controlled synthesis of metal oxide nanostructures.
机译:尽管在过去的十年中已经对无机纳米材料进行了广泛的合成研究,但是快速合成具有高表面积/体积比的晶体微孔纳米结构仍然是一项重大挑战。在这项工作中,我们结合了微波加热和表面活性剂的优异性能,首次开发了一种新型的表面活性剂辅助微波加热途径,用于快速合成对乙醇具有很高敏感性的结晶微孔SnO2。本文研究并讨论了制备的微孔SnO2的形成机理。此外,该合成途径被证明是用于金属氧化物纳米结构的形状控制合成的通用且快速的方法。

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