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首页> 外文期刊>The journal of physical chemistry, C. Nanomaterials and interfaces >Preparation and Characterization of Alane Complexes for Energy Applications
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Preparation and Characterization of Alane Complexes for Energy Applications

机译：能源应用中铝烷配合物的制备与表征

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摘要

Alane (AlH3) has attracted much recent attention for various energy related applications. Amines are commonly used as stabilization agents in alane complexes, with N-methylpyrrolidine (NMP) in particular for favorable properties. However, there have been complications in the study of alane-NMP complexes due to the fact that the widely employed synthesis schemes would produce a mixture of complexes in different compositions. Reported here are the preparation and quantitative characterization of two complexes AlH3·NMP and AlH3·(NMP)2, and also AlH2Cl · (NMP)2 as a product obtained under slightly different reaction conditions. Results on the hydrogen storage capacities in and hydrogen release from these complexes are also reported and discussed.
机译：Alane（AlH3）最近在各种能源相关应用中引起了广泛关注。胺通常用作烷烃络合物中的稳定剂，尤其是与N-甲基吡咯烷酮（NMP）具有良好的性能。然而，由于广泛采用的合成方案将产生不同组成的复合物的混合物，在烷烃-NMP复合物的研究中存在复杂性。本文报道了两种配合物AlH3·NMP和AlH3·（NMP）2的制备和定量表征，以及在略有不同的反应条件下获得的产物AlH2Cl·（NMP）2。还报道和讨论了这些配合物中的氢存储能力和氢释放的结果。

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