Structure and magnetic property of a cobalt(II) complex synthesized through in situ hydrothermal reaction

Liu M.-L.; Fang M.; Zhao B.

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Structure and magnetic property of a cobalt(II) complex synthesized through in situ hydrothermal reaction

机译：原位水热反应合成钴（II）配合物的结构和磁性

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A new cobalt(II) coordination polymer [Co(L_1)(bpy)- (H _2O)].H_2O(1,H_2L_1=2-sulfobenzoic acid and bpy=4,4′-bipyridine) was synthesized by in situ hydrothermal reaction. The single-crystal X- ray diffraction analysis shows that compound 1 belongs to monoclinic system with space group C2/c. The structure of compound 1 exhibits a 2D framework linked by ligand L_1 and 4,4′-bpy, of which L1 was produced by in situ hydrothermal reaction of 2-(pyridinyl-4-methyl- sulfanyl) benzoic acid. The 2D structure was future connected into a 3D framework through hydrogen bonds. The magnetic analysis indicates the presence of weakly antiferromagnetic interaction between adjacent Co~(2+).

机译：通过原位水热反应合成了一种新型的钴（II）配位聚合物[Co（L_1）（bpy）-（H _2O）.H_2O（1，H_2L_1 = 2-磺基苯甲酸和bpy = 4,4'-联吡啶）。 X射线单晶衍射分析表明，化合物1属于单斜晶系，空间群为C2 / c。化合物1的结构表现出由配体L_1和4,4'-bpy连接的2D骨架，其中L1是通过2-（吡啶基-4-甲基-硫烷基）苯甲酸的原位水热反应产生的。将来2D结构通过氢键连接到3D框架中。磁性分析表明相邻的Co〜（2+）之间存在弱反铁磁相互作用。

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《Zeitschrift fur Anorganische und Allgemeine Chemie》 |2009年第15期|共4页
作者
Liu M.-L.; Fang M.; Zhao B.;
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正文语种 eng
中图分类化学;
关键词
Cobalt(II) complex; Crystal structure; In situ reaction; Magnetic properties; X-ray diffraction;

机译：钴（II）配合物;晶体结构;原位反应;磁性;X射线衍射;

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1. Structure and magnetic property of a cobalt(II) complex synthesized through in situ hydrothermal reaction [J] . Liu M.-L., Fang M., Zhao B. Zeitschrift fur Anorganische und Allgemeine Chemie . 2009,第15期

机译：原位水热反应合成钴（II）配合物的结构和磁性
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Structure and magnetic property of a cobalt(II) complex synthesized through in situ hydrothermal reaction

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