Four new compounds based on terephthalate and 2-(4-Pyridyl)benzimidazole ligands

Xia C.-K.; Wu Y.-L.; Xie J.-M.

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Four new compounds based on terephthalate and 2-(4-Pyridyl)benzimidazole ligands

机译：四种基于对苯二甲酸酯和2-（4-吡啶基）苯并咪唑配体的新化合物

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摘要

Four new compounds based on H_2BDC and PyBIm [H2BDC = 1,4-benzenedicarboxylatic acid, PyBIm = 2-(4-pyridyl)benzimidazole], (PyBIm)(H_2BDC)_(0.5) (1), Co(PyBIm)_2(HBDC)(BDC) _(0.5) (2), Ni(PyBIm)_2(HBDC)(BDC)_(0.5) (3), and Zn(BDC)(PyBIm) ·H_2O (4), were synthesized by hydrothermal methods and characterized by X-ray diffraction. Compound 1 contains two types of hydrogen bonding N-H?N and O-HA?N, which connect the molecules into a two-dimensional (2D) layer. Complex 2 crystallizes isostructural to 3 in triclinic space group P|{1}, in 1D chains. The hydrogen-bonding interactions between uncoordinated N, N-H and COOH groups in 2 connect the 1D chains into a 2D layer. Complex 4 displays a 1D structure, which is finally extended to a 3D supramolecular framework by hydrogen bonding and π-π packing interactions. The magnetic properties of compounds 2 and 3 were studied as well.

机译：四种基于H_2BDC和PyBIm的新化合物[H2BDC = 1,4-苯二甲酸，PyBIm = 2-（4-吡啶基）苯并咪唑]，（PyBIm）（H_2BDC）_（0.5）（1），Co（PyBIm）_2（水热法合成HBDC）（BDC）_（0.5）（2），Ni（PyBIm）_2（HBDC）（BDC）_（0.5）（3）和Zn（BDC）（PyBIm）·H_2O（4）方法，并通过X射线衍射进行表征。化合物1包含两种类型的氢键N-H2N和O-HA2N，它们将分子连接成二维（2D）层。一维链中的三斜体空间群P | {1}中，复合物2结晶为3。 2中未配位的N，N-H和COOH基团之间的氢键相互作用将1D链连接到2D层中。配合物4显示1D结构，最后通过氢键和π-π堆积相互作用扩展到3D超分子框架。还研究了化合物2和3的磁性。

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《Zeitschrift fur Anorganische und Allgemeine Chemie》 |2011年第2期|共7页
作者
Xia C.-K.; Wu Y.-L.; Xie J.-M.;
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正文语种 eng
中图分类化学;
关键词
Benzimidazoles; Cobalt; Magnetic properties; Nickel; Terephthalates; Zinc;

机译：苯并咪唑;钴;磁性;镍;对苯二甲酸;锌;

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专利

1. Four new compounds based on terephthalate and 2-(4-Pyridyl)benzimidazole ligands [J] . Xia C.-K., Wu Y.-L., Xie J.-M. Zeitschrift fur Anorganische und Allgemeine Chemie . 2011,第2期

机译：四种基于对苯二甲酸酯和2-（4-吡啶基）苯并咪唑配体的新化合物
2. COBALT-MEDIATED SYNTHESIS OF 2-(4-PYRIDYL) BENZIMIDAZOLE. X-RAY STRUCTURES OF CO[2-(4-PYRIDYL)BENZIMIDAZOLE]_2(H_2O)_2(NO_3)_2 AND [CO(ISONICOTINATE)(4-PYRIDNIUMCARBOXYLATE)(H_2O)(NO_3)]_(propor. to) [J] . Zhiyong Wang, Scott R. Wilson, Bruce M. Foxman, Crystal engineering . 1999,第2a3期

机译：钴介导的2-（4-吡啶基）苯并咪唑的合成。 CO [2-（4-吡啶基）苯并咪唑] _2（H_2O）_2（NO_3）_2和[CO（异烟酸酯）（4-吡啶甲酸羧酯）（H_2O）（NO_3）] _（的比例）的X射线结构
3. A new Co(II) coordination polymer with the 2-(4-pyridyl)-terephthalate ligand: synthesis, crystal structure and magnetic properties [J] . Tian Danian, Ding Runmei, Chen Bingbing, Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences . 2019,第7a8期

机译：具有2-（4-吡啶基）的新CO（II）配位聚合物 - 对苯二甲酸酯配体：合成，晶体结构和磁性
4. Syntheses, Crystal Structures and Luminescence of Two Coordination Polymers Based on Isophthalic Acid and 2-(3-Pyridyl)benzimidazole Ligands [C] . Kefen Yue, Shuang Zhao, Ruili Zhao International Conference on Chemical, Material and Metallurgical Engineering . 2012

机译：基于间苯二甲酸和2-（3-吡啶基）苯并咪唑配体的两种配位聚合物的合成，晶体结构和发光
5. Synthesis and photoluminescent properties of linear and starburst compounds based on benzimidazole, 2-(2'-pyridyl)benzimidazole and 2,2'-dipyridylamine [D] . White, Wade M. 2007

机译：基于苯并咪唑，2-（2'-吡啶基）苯并咪唑和2,2'-二吡啶胺的直链和星暴化合物的合成和光致发光性质
6. Role of the Metal Center in the Modulation of the Aggregation Process of Amyloid Model Systems by Square Planar Complexes Bearing 2-(2′-pyridyl)benzimidazole Ligands [O] . Daniele Florio, Ilaria Iacobucci, Giarita Ferraro, 2019

机译：金属中心在带有2-（2-吡啶基）苯并咪唑配体的方形平面络合物对淀粉样蛋白模型系统聚集过程的调控中的作用
7. Development of 2-(4-pyridyl)-benzimidazoles as PKN2 chemical tools to probe cancer [O] . Fiona Scott, Angela M. Fala, Lewis E. Pennicott, 2020

机译：发展2-（4-吡啶基）-Benzimidazoles作为PKN2化学工具探测癌症

Four new compounds based on terephthalate and 2-(4-Pyridyl)benzimidazole ligands

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