BI24RU3BR20 - A PSEUDO-TETRAGONAL STRUCTURE WITH [RUBI6BR12] CLUSTERS AND [RU2BI17BR4] GROUPS [German]

Ruck M.

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BI24RU3BR20 - A PSEUDO-TETRAGONAL STRUCTURE WITH [RUBI6BR12] CLUSTERS AND [RU2BI17BR4] GROUPS [German]

机译：BI24RU3BR20-具有[RUBI6BR12]簇和[RU2BI17BR4]组[德国]的拟四边形结构

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The melting reaction of Ru with Bi and BiBr yields black, lustrous, air insensitive crystals of the subbromide Bi24Ru3Br20. The orthorhombic crystal structure (space group Pc2(1)n, a = b = 1377.8(1) pm, c = 3222.3(4) pm, V = 6117.0.10(6) pm(3)) deceives pseudo-symmetry with respect to the tetragonal space group P4cc leading to multiply twinned crystals. The structure can formally be subdivided in [RuBi6Br12] clusters, [Ru2Bi17Br4] stacks, and [BiBr4] groups. [References: 29]

机译：Ru与Bi和BiBr的熔融反应生成亚溴化Bi24Ru3Br20黑色，有光泽，对空气不敏感的晶体。正交晶体结构（空间群Pc2（1）n，a = b = 1377.8（1）pm，c = 3222.3（4）pm，V = 6117.0.10（6）pm（3））相对于伪对称性到四边形空间群P4 / ncc导致多重孪晶的形成。可以将结构正式细分为[RuBi6Br12]簇，[Ru2Bi17Br4]堆栈和[BiBr4]组。 [参考：29]

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《Zeitschrift fur Anorganische und Allgemeine Chemie》 |1997年第10期|共8页
作者
Ruck M.;
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正文语种 ger
中图分类化学;
关键词
Bismuth ruthenium bromide; Subhalide; Cluster; Crystal structure; Pseudo-symmetry; Twinning; Transition-metals; Iodide clusters; Encapsulation;

机译：溴化铋铋;亚卤化物;簇;晶体结构;拟对称;孪生;过渡金属;碘化物簇;包封;

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1. BI24RU3BR20 - A PSEUDO-TETRAGONAL STRUCTURE WITH [RUBI6BR12] CLUSTERS AND [RU2BI17BR4] GROUPS [German] [J] . Ruck M. Zeitschrift fur Anorganische und Allgemeine Chemie . 1997,第10期

机译：BI24RU3BR20-具有[RUBI6BR12]簇和[RU2BI17BR4]组[德国]的拟四边形结构
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BI24RU3BR20 - A PSEUDO-TETRAGONAL STRUCTURE WITH [RUBI6BR12] CLUSTERS AND [RU2BI17BR4] GROUPS [German]

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