Synthesis and characterization of a H+ exchanged zirconate

Orera A; Kuhn A; Alvarado FG

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Synthesis and characterization of a H+ exchanged zirconate

机译：H +交换锆酸酯的合成与表征

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A new protonated oxide has been synthesized by ion exchange of lithium by proton in lithium metazirconate, Li2ZrO3. Easy and complete ion exchange has been achieved in acidic medium. Characterization of the protonated solid by means of X-ray powder diffraction and thermogravimetric analysis allow to propose the nominal formulation "H2ZrO3". However vibrational spectroscopy suggests that a more appropriate formulation would be as an oxyhydroxide ZrO(OH)(2).

机译：通过在偏锆酸锂Li2ZrO3中进行质子与锂的离子交换，合成了一种新的质子化氧化物。在酸性介质中已经实现了简单而完整的离子交换。通过X射线粉末衍射和热重分析对质子化的固体进行表征，可以提出标称配方“ H2ZrO3”。但是，振动光谱表明，更合适的配方应为羟基氧化ZrO（OH）（2）。

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《Zeitschrift fur Anorganische und Allgemeine Chemie》 |2005年第11期|共3页
作者
Orera A; Kuhn A; Alvarado FG;
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正文语种 eng
中图分类化学;
关键词
lithium zirconate; ion exchange; proton exchange; zirconium dioxide; THERMAL-DECOMPOSITION; ZRO2; PH;

机译：锆酸锂;离子交换;质子交换;二氧化锆;热分解;ZRO2;PH;

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1. Synthesis and characterization of a H+ exchanged zirconate [J] . Orera A, Kuhn A, Alvarado FG Zeitschrift fur Anorganische und Allgemeine Chemie . 2005,第11期

机译：H +交换锆酸酯的合成与表征
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机译：锆酸盐耐火材料。第2部分：锶，锆酸盐，锆酸钙和锆酸钡的合成和一些性质

Synthesis and characterization of a H+ exchanged zirconate

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