Synthesis, characterization, and crystal structure of a new coordination polymer of lead(II) containing 2,6-pyridinedicarboxylic acid

Rafizadeh M; Amani V; Neumuller B

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Synthesis, characterization, and crystal structure of a new coordination polymer of lead(II) containing 2,6-pyridinedicarboxylic acid

机译：新型含2,6-吡啶二羧酸铅（II）配位聚合物的合成，表征和晶体结构

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The reaction of solution 2,6-pyridinedicarboxylic acid (1) and 2,2'-Bipyridine with Pb(NO3)(2) led to the coordination polymer [Pb(pydc)](n) (2) (pydcH(2) is 2,6-pyridinedicarboxylic acid). This complex was characterized by elemental analysis, IR spectroscopy and sin : ale-crystal structure of 2. Crystal data for 2 at -80 degrees C: monoclinic, space group P2(1), a = 977.2(1), b = 554.0(1), c = 1425.3(2)pm, beta = 104.75(1)degrees, Z = 4, R-1 = 0.0261. The units [Pb(pyde)] form infinite chains along [010].

机译：溶液2,6-吡啶二羧酸（1）和2,2'-联吡啶与Pb（NO3）（2）的反应生成配位聚合物[Pb（pydc）]（n）（2）（pydcH（2）是2,6-吡啶二羧酸）该配合物的特征在于元素分析，红外光谱和sin：2的易结晶结构。-80°C下2的晶体数据：单斜晶系，空间群P2（1）/ n，a = 977.2（1），b = 554.0（1），c = 1425.3（2）pm，beta = 104.75（1）度，Z = 4，R-1 = 0.0261。 [Pb（pyde）]单位沿[010]形成无限链。

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《Zeitschrift fur Anorganische und Allgemeine Chemie》 |2006年第15期|共2页
作者
Rafizadeh M; Amani V; Neumuller B;
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正文语种 eng
中图分类化学;
关键词
lead(II); 2; 6-pyridinedicarboxylic acid; crystal structure; MONOHYDRATE; COMPLEXES; DIHYDRATE;

机译：铅（II）;2;6-吡啶二甲酸;晶体结构;一水合物;络合物;二水合物;

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1. Synthesis, characterization, and crystal structure of a new coordination polymer of lead(II) containing 2,6-pyridinedicarboxylic acid [J] . Rafizadeh M, Amani V, Neumuller B Zeitschrift fur Anorganische und Allgemeine Chemie . 2006,第15期

机译：新型含2,6-吡啶二羧酸铅（II）配位聚合物的合成，表征和晶体结构
2. Synthesis, Crystal Structures, and Magnetic Properties of Three Cobalt(II) Coordination Polymers Constructed from 3,5-Pyridinedicarboxylic Acid or 3,4-Pyridinedicarboxylic Acid Ligands [J] . Xiaojing Zhou, Xiaolei Guo, Lili Liu, Crystals . 2019,第3期

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3. Synthesis, structures, and photoluminescence properties of three metal(II) coordination polymers derived from a flexible tripodal ligand and 2,6-pyridinedicarboxylic acid [J] . Shi-Meng Wang, Ling Qian, Hong-Ye Bai Transition Metal Chemistry . 2013,第2期

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4. Synthesis, Structures and Properties of Two New Three-dimensional Ce(III) Coordination Polymers with 2,2'-bipyridine-4,4'-dicarboxylic Acid [C] . Ruiping Zheng, Huiyuan Chen, Junjie He, International Conference on Advanced Engineering Materials and Technology . 2013

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机译：包含多个对芳基氮杂或对苯二甲二亚胺基团的单体和聚合物的合成和表征：导电聚合物，液晶聚合物和二元聚合物。
6. Hydrothermal synthesis and crystal structure of a new lanthanum(III) coordination polymer with fumaric acid [O] . Hayet Anana, Chahrazed Trifa, Sofiane Bouacida, 2015

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7. Synthesis, Crystal Structures, and Magnetic Properties of Three Cobalt(II) Coordination Polymers Constructed from 3,5-Pyridinedicarboxylic Acid or 3,4-Pyridinedicarboxylic Acid Ligands [O] . Xiaojing Zhou, Xiaolei Guo, Lili Liu, 2019

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8. Model Compound Studies of Rigid Rod Aromatic Heterocyclic Polymer Systems, the X-Ray Crystal Structure of 2,6-Diphenylbenzo (1,2-d; 5,4-d') Diimidazole Tetrahydrate, C2OH14N4. 4H2O, a Model System for the Study of Polymer-Water Interaction in Polybenzimidazoles. [R] . Hunsaker, M., Adams, W. W., Fratini, A. V. 1983

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Synthesis, characterization, and crystal structure of a new coordination polymer of lead(II) containing 2,6-pyridinedicarboxylic acid

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