One-pot multicomponent synthesis of furo[3,2-c]coumarins promoted by amino-functionalized Fe3O4@SiO2 nanoparticles

Safaei-Ghomi Javad; Shahbazi-Alavi Hossein; Babaei Pouria

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One-pot multicomponent synthesis of furo[3,2-c]coumarins promoted by amino-functionalized Fe3O4@SiO2 nanoparticles

机译：氨基官能化的Fe3O4 @ SiO2纳米颗粒促进一锅多组分合成呋喃并[3,2-c]香豆素

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Amino-functionalized Fe3O4@SiO2 nanoparticles (Fe3O4@SiO2-NH2 NPs) were prepared by treating Fe3O4@ SiO2 NPs with (3-aminopropyl)-triethoxysilane. They have been characterized by powder X-ray diffraction, vibrating sample magnetometer, scanning electronic microscopy, energy dispersive X-ray, thermogravimetric analysis and FT-IR spectroscopy. A neat, atom-economical, environmentally benign one-pot multicomponent synthetic route for the synthesis of furo[3,2-c] coumarins in good yields has been devised using the Fe3O4@SiO2-NH2 NPs. The present methodology can be used for the design of libraries and diversity-oriented synthesis, and has potential for biological applications and drug discovery.

机译：通过用（3-氨基丙基）-三乙氧基硅烷处理Fe3O4 @ SiO2 NPs，制备了氨基官能化的Fe3O4 @ SiO2纳米颗粒（Fe3O4 @ SiO2-NH2 NPs）。它们的特征在于粉末X射线衍射，振动样品磁力计，扫描电子显微镜，能量色散X射线，热重分析和FT-IR光谱。使用Fe3O4 @ SiO2-NH2 NPs，已经设计了一种整齐的，原子经济的，环境友好的多锅合成路线，可以高收率合成呋喃[3,2-c]香豆素。本方法学可用于文库的设计和面向多样性的合成，并具有生物应用和药物发现的潜力。

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《Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences》 |2016年第8期|共8页
作者
Safaei-Ghomi Javad; Shahbazi-Alavi Hossein; Babaei Pouria;
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正文语种 eng
中图分类化学;
关键词
amino-functionalized Fe3O4@SiO2 nanoparticles; furo3; 2-ccoumarins; multicomponent; nanocatalyst; one-pot;

机译：氨基官能化Fe3O4 @ SiO2纳米颗粒;呋喃[3;2-c]香豆素;多组分;纳米催化剂;一锅法;

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1. One-pot multicomponent synthesis of furo[3,2-c]coumarins promoted by amino-functionalized Fe3O4@SiO2 nanoparticles [J] . Safaei-Ghomi Javad, Shahbazi-Alavi Hossein, Babaei Pouria Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences . 2016,第8期

机译：氨基官能化的Fe3O4 @ SiO2纳米颗粒促进一锅多组分合成呋喃并[3,2-c]香豆素
2. Catalyst-Free One-Pot Synthesis of Novel Heteroarylamine Substituted Furo[3,2-c ]coumarins [J] . Olyaei Abolfazl, Saraei Mahnaz, Khoeiniha Reyhaneh Synlett . 2018,第12期

机译：新型杂芳基胺取代呋喃的催化剂单罐合成[3,2-C]香豆素
3. DABCO-catalysed one-pot synthesis of Furo[3,2-c]coumarin from 3-halochromone [J] . Sourav Maiti, Jaydip Ghosh, Tapas Sarkar Journal of the Indian Chemical Society . 2013,第9期

机译：DABCO催化由3-卤代色酮一锅合成呋喃[3,2-c]香豆素
4. ONE-POT MULTICOMPONENT SYNTHESIS of 3,4-DIHYDROPYRIMIDIN-2(1H)-ONES USING SILICA-SUPPORTED PREYSSLER NANOPARTICLES AS A NOVEL, ECO-FRIENDLY and GREEN CATALYST [C] . Fatemeh F. Bamoharram, Majid M. Heravi, Mina Roshani, 6th international conference on environmental catalysis : Abstract book . 2010

机译：一键多组分合成3,4-二氢吡啶酮N-2（1H）-使用二氧化硅支撑的PreySSLer纳米粒子作为新型，环保和绿色催化剂
5. Nanoparticle Formation in the Flame Synthesis of Multicomponent Nanostructured Materials for Clean Energy Applications [D] . Fang, Jiaxi. 2016

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6. A One-pot Condensation for Synthesis 2-methyl-4-phenylpyrano3 2-c chromen-5(4H)-one and Synthesis of Warfarin by Ionic Liquid Catalysis [O] . Aazam Monfared, Zohreh Esmaeeli 2016

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7. VCl3-catalyzed aza-Diels-Alder reaction: one-pot synthesis of pyrano[3,2-c]- and furo[3,2-c]quinolines [O] . Gowravaram Sabitha, M. Shashi Kumar Reddy, K. Arundhathi, 2006

机译：VCl3催化的氮杂-Diels-alder反应：一锅法合成吡喃[3,2-c] - 和呋喃[3,2-c]喹啉

One-pot multicomponent synthesis of furo[3,2-c]coumarins promoted by amino-functionalized Fe3O4@SiO2 nanoparticles

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