Direct Oxidative Deprotection of Trimethylsilyl and Tetrahydropyranyl Ethers Using Alumina-Supported Iodobenzene Diacetate under Non-Aqueous Conditions

Majid M. Heravi; Mahmood Tajbakhsh; Mitra Ghassemzadeh

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Direct Oxidative Deprotection of Trimethylsilyl and Tetrahydropyranyl Ethers Using Alumina-Supported Iodobenzene Diacetate under Non-Aqueous Conditions

机译：氧化铝负载的碘代苯二乙酸酯在非水条件下对三甲基甲硅烷基和四氢吡喃基醚的直接氧化脱保护

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摘要

Primary and secondary trimethylsilyl and tetrahydropyranyl ethers are converted to their carbonyl compounds efficiently using alumina-supported iodobenzene diacetate.

机译：使用氧化铝负载的碘代苯二乙酸酯可将伯和仲三甲基甲硅烷基和四氢吡喃基醚有效地转化为羰基化合物。

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《Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences》 |1999年第3期|共3页
作者
Majid M. Heravi; Mahmood Tajbakhsh; Mitra Ghassemzadeh;
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正文语种 eng
中图分类化学;
关键词
trimethylsilyl ethers; tetrahydropyranyl ethers; alumina-supported iodobenzene diacetate;

机译：三甲基甲硅烷基醚;四氢吡喃基醚;氧化铝负载的碘代苯二乙酸酯;

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1. Direct Oxidative Deprotection of Trimethylsilyl and Tetrahydropyranyl Ethers Using Alumina-Supported Iodobenzene Diacetate under Non-Aqueous Conditions [J] . Majid M. Heravi, Mahmood Tajbakhsh, Mitra Ghassemzadeh Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences . 1999,第3期

机译：氧化铝负载的碘代苯二乙酸酯在非水条件下对三甲基甲硅烷基和四氢吡喃基醚的直接氧化脱保护
2. Benzyltriphenylphosphonium chlorate (BTPPC) as a new and mild reagent for oxidative deprotection of trimethylsilyl and tetrahydropyranyl ethers of benzylic alcohols under non-aqueous conditions [J] . Hajipour AR., Mallakpour SE., Mohammadpoor-Baltork I., Tetrahedron . 2002,第1期

机译：氯苄基三苯基氯phosph（BTPPC）作为一种新型的温和试剂，可在非水条件下氧化脱保护苄醇的三甲基甲硅烷基和四氢吡喃基醚
3. Benzyltriphenylphosphonium peroxodisulfate: a mild and inexpensive reagent for selective oxidative deprotection of trimethylsilyl and tetrahydropyranyl ethers, ethylene acetals and ketals under non-aqueous and aprotic conditions [J] . Mahmood Tajbakhsh, Iraj Mohammadpoor-Baltork, Farhad Ramzanian-Lehmali Journal of Chemical Research. Synopses . 2001,第5期

机译：过氧二硫酸苄基三苯基phosph：一种温和且便宜的试剂，用于在非水和非质子条件下对三甲基甲硅烷基和四氢吡喃基醚，乙缩醛和缩酮进行选择性氧化脱保护
4. Manganeseporphyrin Catalyzed Hydrocarbons Oxidation by Iodobenzene Diacetate in Ionic Liquid at Room Temperature [C] . Z. Li, C.G Xia Asia-Pacific Congress on Catalysis . 2003

机译：Manganesehorphyrin催化碳氢化合物通过碘苯乙酸在室温下在离子液中氧化
5. Part I. Asymmetric organocatalysis: (1) Direct enantioselective organocatalytic hydroxymethylation of aldehydes catalyzed by alpha,alpha-diphenylprolinol trimethylsilyl ether: Application in the formal synthesis of (-)-Rasfonin; (2) Synthesis of a novel bicyclic secondary amine organocatalyst: Application to the direct enantioselective organocatalytic hydroxymethylation of aldehydes. Part II. Asymmetric synthesis of bicyclic analogues of the anti-osteoporotic drug risedronate. [D] . Miller, John Robert. 2010

机译：第一部分，不对称有机催化：（1）α，α-二苯基脯氨醇三甲基甲硅烷基醚催化的醛的直接对映选择性有机催化羟甲基化：在（-）-Rasfonin的正式合成中的应用；（2）新型双环仲胺有机催化剂的合成：应用于醛的直接对映选择性有机催化羟甲基化。第二部分抗骨质疏松药物Risedronate的双环类似物的不对称合成。
6. Ladder Polyether Synthesis via Epoxide-Opening Cascades Directed by a Disappearing Trimethylsilyl Group [O] . Timothy P. Heffron, Graham L. Simpson, Estibaliz Merino, -1

机译：梯子通过环氧基团的开幕瀑布导演聚醚合成消失的三甲基硅基
7. An Efficient Method for Selective Deprotection of Trimethylsilyl Ethers and Tetrahydropyranyl Ethers under Solvent-free Conditions [O] . 2005

机译：在无溶剂条件下选择性脱保护三甲基甲硅烷基醚和四氢吡喃基醚的有效方法

Direct Oxidative Deprotection of Trimethylsilyl and Tetrahydropyranyl Ethers Using Alumina-Supported Iodobenzene Diacetate under Non-Aqueous Conditions

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