Coordination between [H_2P_2W_(12)O _(48)]~(12-) and antimony(iii): Synthesis and characterization of sandwich complex derived from the new f>O_(51)} fragment

Zhang C.-D.; Liu S.-X.; Ma F.-J.; Tan R.-K.; Zhang W.; Su Z.-M.

首页> 外文期刊>Dalton transactions: An international journal of inorganic chemistry >Coordination between [H_2P_2W_(12)O _(48)]~(12-) and antimony(iii): Synthesis and characterization of sandwich complex derived from the new f>O_(51)} fragment

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Coordination between [H_2P_2W_(12)O _(48)]~(12-) and antimony(iii): Synthesis and characterization of sandwich complex derived from the new f>O_(51)} fragment

机译：[H_2P_2W_（12）O _（48）]〜（12-）与锑（iii）之间的配位：源自新的f> O_（51）}片段的三明治复合物的合成与表征

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A sandwich-type anionic cluster of a new lacunary building block [P _2W_(13)O_(51)]~(14-) has been prepared: [H_6{P_2W_(13)O_(51)}_2Sb _4]~(10-) (1) was synthesized in a one-pot self-assembly reaction of [H_2P_2W_(12)O_(48)] ~(12-) with C_4H_4KO_7Sb·0.5H _2O and characterized by single-crystal X-ray analysis, IR, thermogravimetric analysis, elemental analysis, UV, NMR and electrochemistry. 1 represents the first dimetric, antimony-containing polyoxoanion derived from a vacant Dawson-type tungstophosphate.

机译：制备了新的湖泊结构单元[P _2W_（13）O_（51）]〜（14-）的三明治型阴离子簇：[H_6 {P_2W_（13）O_（51）} _ 2Sb _4]〜（10 -）（1）在[H_2P_2W_（12）O_（48）]〜（12-）与C_4H_4KO_7Sb·0.5H _2O的一锅自组装反应中合成，并通过单晶X射线分析，IR表征，热重分析，元素分析，UV，NMR和电化学。图1表示衍生自空的Dawson型钨磷酸盐的第一二等分的含锑的聚氧阴离子。

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《Dalton transactions: An international journal of inorganic chemistry》 |2010年第34期|共5页
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Zhang C.-D.; Liu S.-X.; Ma F.-J.; Tan R.-K.; Zhang W.; Su Z.-M.;
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机译：[H_2P_2W_（12）O _（48）]〜（12-）与锑（iii）之间的配位：源自新的f> O_（51）}片段的三明治复合物的合成与表征
2. Coordination Chemistry of the Hexavacant Tungstophosphate [H2P2W12O48]12- with FeIII Ions: Towards Original Structures of Increasing Size and Complexity [J] . Beatrice Godin, Ya-Guang Chen, Jacqueline Vaissermann, Angewandte Chemie . 2005,第20期

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Coordination between [H_2P_2W_(12)O _(48)]~(12-) and antimony(iii): Synthesis and characterization of sandwich complex derived from the new f>O_(51)} fragment

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