Solvothermal synthesis and characterization of two inorganic-organic hybrid materials based on barium

Abdollahian Y.; Hauser J.L.; Rogow D.L.; Oliver A.G.; Oliver S.R.J.

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Solvothermal synthesis and characterization of two inorganic-organic hybrid materials based on barium

机译：两种基于钡的无机-有机杂化材料的溶剂热合成与表征

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Two metal-organic frameworks containing barium were synthesized hydrothermally and investigated for their catalytic properties. Ba _2F _2[O _3SC _2H _4SO _3] has barium fluoride layers linked by organic 1,2-ethanedisulfonate molecules. Ba[O _3SC _2H _4SO _3] has discrete barium centers arranged in layers and connected covalently by ethanedisulfonate bridges. Thermogravimetric analysis showed that Ba _2F _2[O _3SC _2H _4SO _3] is stable to ca. 325 °C and Ba[O _3SC _2H _4SO _3] to ca. 375 °C. These materials expand the metal-organic frameworks available for group II metals bound to organodisulfonate linkers and are potentially useful for a range of heterogeneous acid catalysis reactions.

机译：水热合成了两种含钡的金属有机骨架，并对其催化性能进行了研究。 Ba _2F _2 [O _3SC _2H _4SO _3]具有由有机1,2-乙烷二磺酸盐分子连接的氟化钡层。 Ba [O _3SC _2H _4SO _3]具有离散的钡中心，钡中心分层排列并通过乙烷二磺酸盐桥共价连接。热重分析表明，Ba _2F _2 [O _3SC _2H _4SO _3]对Ca稳定。 325°C，Ba [O _3SC _2H _4SO _3]至约。 375℃。这些材料扩展了可用于结合到有机二磺酸盐连接基的II族金属的金属-有机骨架，并可能用于多种异质酸催化反应。

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《Dalton transactions: An international journal of inorganic chemistry》 |2012年第40期|共5页
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Abdollahian Y.; Hauser J.L.; Rogow D.L.; Oliver A.G.; Oliver S.R.J.;
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Solvothermal synthesis and characterization of two inorganic-organic hybrid materials based on barium

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