A technetium intermediate specifically promotes deprotection of trifluoroacetyl HYNIC during radiolabelling under mild conditions

Surfraz MBU; Biagini SCG; Blower PJ

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A technetium intermediate specifically promotes deprotection of trifluoroacetyl HYNIC during radiolabelling under mild conditions

机译：mild中间体在温和条件下的放射性标记过程中特别促进三氟乙酰基HYNIC的脱保护

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摘要

The trifluoroacetyl group protects the nucleophilic HYNIC from unwanted side reactions yet allows radiolabelling with technetium-99m under mild conditions, due to efficient and specific promotion of deprotection by a technetium complex intermediate.

机译：三氟乙酰基可保护亲核HYNIC免受有害副反应的影响，但由于mild络合物中间体的高效脱保护作用，可在温和条件下用tech 99m进行放射性标记。

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《Dalton transactions: An international journal of inorganic chemistry》 |2008年第22期|共3页
作者
Surfraz MBU; Biagini SCG; Blower PJ;
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正文语种 eng
中图分类无机化学;
关键词
RAY CRYSTAL-STRUCTURE; IMAGING FOCAL SITES; PROTEIN-BINDING; TC-99M; PEPTIDE; COMPLEXES; INFECTION; RADIOPHARMACEUTICALS; POLYPEPTIDES; ANTAGONIST;

机译：射线晶体结构;成像部位;蛋白质结合;TC-99M;肽;复合物;感染;放射性药物;多肽;拮抗剂;

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专利

1. A technetium intermediate specifically promotes deprotection of trifluoroacetyl HYNIC during radiolabelling under mild conditions [J] . Surfraz MBU, Biagini SCG, Blower PJ Dalton transactions: An international journal of inorganic chemistry . 2008,第22期

机译：mild中间体在温和条件下的放射性标记过程中特别促进三氟乙酰基HYNIC的脱保护
2. Technetium-99m-labeled liposomes to image experimental colitis in rabbits: comparison with technetium-99m-HMPAO-granulocytes and technetium-99m-HYNIC-IgG. [J] . Dams ET, Oyen WJ, Boerman OC, The Journal of Nuclear Medicine . 1998,第12期

机译：net 99m标记的脂质体可在家兔的实验性结肠炎中成像：与tech 99m-HMPAO-粒细胞和tech 99m-HYNIC-IgG的比较。
3. Efficient [3,3]-sigmatropic rearrangement accelerated by a trifluoroacetyl group: synthesis of benzofurans under mild conditions [J] . Okiko Miyata, Norihiko Takeda, Yoshiaki Morikami, Organic & biomolecular chemistry . 2003,第2期

机译：三氟乙酰基促进的高效[3,3]-σ重排：在温和条件下合成苯并呋喃
4. New Mild Deprotection Method of the 2,2,2 - Trichloroethoxycarbonyl (TROC) Group whit Mischmetal(Abstracts) [C] . Vellemae Eerold, Lebedev Oleg, Maeorg Uno European Symposium on Organic Chemistry . 2007

机译：2,2,2-三氯乙氧基羰基（TROC）组丝毫模糊的新的轻度脱保护方法（摘要）
5. I. Tertiary aryl sulfonamides as new cross coupling partners for nickel catalyzed Kumada-Corriu-Tamao reductive and carbon-carbon bond forming cross coupling reactions. II. N-sulfonyl deprotection under mild nickel(0) catalyzed Kumada-Corriu-Tamao coupling conditions and development of the N-Ans protecting group. III. Synthesis and application of 3,3'-di-(2-pyridyl)-1,1'-bi-2-naphthol ligands [D] . Milburn, Robert Ronald 2004

机译：I.叔芳基磺酰胺作为镍催化的Kumada-Corriu-Tamao还原和碳-碳键形成交叉偶联反应的新交叉偶联伴侣。二。在温和的镍（0）下N-磺酰基脱保护催化了Kumada-Corriu-Tamao偶联条件和N-Ans保护基的发展。三， 3,3'-二-（2-吡啶基）-1,1'-bi-2-萘酚配体的合成及应用
6. Cholecystokinin-2 Receptor Targeting with Novel C-terminally Stabilized HYNIC-Minigastrin Analogs Radiolabeled with Technetium-99m [O] . Maximilian Klingler, Christine Rangger, Dominik Summer, 2019

机译：Tech标记99m的新型C末端稳定的HYNIC-Minigastrin类似物靶向的胆囊收缩素2受体。
7. Evaluation of radiolabelled hynic-salmon calcitonin analogues as imaging agents for multiple myeloma and characterisation of novel hynic derivatives as chelators for technetium [O] . Meszaros Levente 2013

机译：放射性标记的hy-鲑鱼降钙素类似物作为多发性骨髓瘤的显像剂的评价和新型ization衍生物的螯合剂表征

A technetium intermediate specifically promotes deprotection of trifluoroacetyl HYNIC during radiolabelling under mild conditions

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